A wedge-mounting technique for nanoscale electron backscatter diffraction

被引：33
作者：
Carpenter, J. S. [1 ]
McCabe, R. J. [1 ]
Beyerlein, I. J. [1 ]
Wynn, T. A. [1 ]
Mara, N. A. [1 ]
机构：
[1] Los Alamos Natl Lab, Los Alamos, NM 87545 USA
来源：
JOURNAL OF APPLIED PHYSICS | 2013年 / 113卷 / 09期
关键词：
TEXTURE EVOLUTION; ROLLING TEXTURES; NANOLAMELLAR COMPOSITES; NEUTRON-DIFFRACTION; BIMETAL INTERFACES; DEFORMATION; COPPER; ORIENTATION; ALLOYS; SLIP;
D O I：
10.1063/1.4794388
中图分类号：
O59 [应用物理学];
学科分类号：
摘要：
The practical spatial resolution of electron backscatter diffraction (EBSD) is around 100 nm, which limits the length scales from which phase and orientation relationship characterization can be accomplished. This precludes collection of statistically relevant data on the crystallography of interfaces within nanomaterials where such information is essential for understanding the unique properties of these materials. In this work, we present a wedge-mounting technique that enables EBSD data to be collected for sub-100 nm thick layers of Cu-Nb bimetallic multilayers fabricated via accumulative roll bonding. We present statistics on layer thickness distributions, grain morphology, orientation distributions, twin volume fraction, and interface character for material with an averaged layer thickness of 86 and 56 nm. (C) 2013 American Institute of Physics. [http://dx.doi.org/10.1063/1.4794388]
引用
收藏
页数：6
相关论文
共 28 条
  • [1] High Resolution EBSD-Based Dislocation Microscopy
    Adams, B. L.
    Fullwood, D. T.
    Basinger, J.
    Hardin, T.
    [J]. TEXTURES OF MATERIALS, PTS 1 AND 2, 2012, 702-703 : 11 - 17
  • [2] Modeling of texture evolution in copper under equal channel angular pressing
    Baik, SC
    Estrin, Y
    Hellmig, RJ
    Jeong, HT
    Brokmeier, HG
    Kim, HS
    [J]. ZEITSCHRIFT FUR METALLKUNDE, 2003, 94 (11): : 1189 - 1198
  • [3] Structure-Property-Functionality of Bimetal Interfaces
    Beyerlein, I. J.
    Mara, N. A.
    Wang, J.
    Carpenter, J. S.
    Zheng, S. J.
    Han, W. Z.
    Zhang, R. F.
    Kang, K.
    Nizolek, T.
    Pollock, T. M.
    [J]. JOM, 2012, 64 (10) : 1192 - 1207
  • [4] Texture evolution via combined slip and deformation twinning in rolled silver-copper cast eutectic nanocomposite
    Beyerlein, Irene J.
    Mara, Nathan A.
    Bhattacharyya, Dhriti
    Alexander, David J.
    Necker, Carl T.
    [J]. INTERNATIONAL JOURNAL OF PLASTICITY, 2011, 27 (01) : 121 - 146
  • [5] A comparison of texture results obtained using precession electron diffraction and neutron diffraction methods at diminishing length scales in ordered bimetallic nanolamellar composites
    Carpenter, J. S.
    Liu, X.
    Darbal, A.
    Nuhfer, N. T.
    McCabe, R. J.
    Vogel, S. C.
    LeDonne, J. E.
    Rollett, A. D.
    Barmak, K.
    Beyerlein, I. J.
    Mara, N. A.
    [J]. SCRIPTA MATERIALIA, 2012, 67 (04) : 336 - 339
  • [6] Bulk texture evolution of Cu-Nb nanolamellar composites during accumulative roll bonding
    Carpenter, J. S.
    Vogel, S. C.
    LeDonne, J. E.
    Hammon, D. L.
    Beyerlein, I. J.
    Mara, N. A.
    [J]. ACTA MATERIALIA, 2012, 60 (04) : 1576 - 1586
  • [7] Carpenter J. S., INT J PLAST UNPUB
  • [8] Carpenter J. S., PHILOS MAG
  • [9] Design of Stable Nanocrystalline Alloys
    Chookajorn, Tongjai
    Murdoch, Heather A.
    Schuh, Christopher A.
    [J]. SCIENCE, 2012, 337 (6097) : 951 - 954
  • [10] Interface structure and radiation damage resistance in Cu-Nb multilayer nanocomposites
    Demkowicz, M. J.
    Hoagland, R. G.
    Hirth, J. P.
    [J]. PHYSICAL REVIEW LETTERS, 2008, 100 (13)
123