Transition metal ion directed bimetallic macrocyclic complexes

被引：8
|
作者：
Khan, TA [1 ]
Shagufta, M [1 ]
机构：
[1] Aligarh Muslim Univ, Dept Chem, Div Inorgan Chem, Aligarh 202002, Uttar Pradesh, India
来源：
TRANSITION METAL CHEMISTRY | 1999年 / 24卷 / 06期
关键词：
D O I：
10.1023/A:1006991215526
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Template condensation of 1,4-phenylenediamine, formaldehyde, 1,3-diaminopropane and benzil in a 1:4:4:2, molar ratio results in the formation of a new series of binuclear decaazamacrocyclic complexes: dichloro/nitrato [1-phenyl bis(8,9-diphenyl-1,3,7,10,14 pentaazacyclo-pentadeca-7,9-diene) metal (II)], [M2LX4](M = Mn-II, Co-II, Ni-II, Cu-II and Zn-II, X = Cl or NO3), which were characterised by i.r., H-1-n.m.r., e.p.r., u.v-vis. spectral studies, conductivity and magnetic susceptibility measurements. All the complexes show octahedral geometry.
引用
收藏
页码：669 / 671
页数：3
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