Preparation of α-Fe2O3 Nanotubes by Calcination of Electrospun Precursors

被引:3
作者
Liu, Ruijiang [1 ,2 ]
Wang, Qiuju [2 ]
Shen, Xiangqian [2 ]
Yang, Xinchun [2 ]
Wu, Deyan [1 ]
Cui, Xuewen [3 ]
机构
[1] Jiangsu Univ, Sch Pharm, Zhenjiang 212013, Peoples R China
[2] Jiangsu Univ, Inst Adv Mat, Zhenjiang 212013, Peoples R China
[3] Jiangsu Univ, Affiliated Hosp, Zhenjiang 212000, Peoples R China
基金
中国国家自然科学基金;
关键词
alpha-Fe2O3; Nanotube; Electrospinning; Morphology; Preparation; FABRICATION; NANOFIBERS; NANOMATERIALS; GROWTH; METAL;
D O I
10.1166/jnn.2014.8477
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The alpha-Fe2O3 nanotubes with diameters of 400-700 nm were prepared by calcination of electrospun precursors. The morphology of alpha-Fe2O3 nanotubes is mainly influenced by the water content in solution and heating rate during the calcination process. When the water content is about 17 wt.%, heating rate is 5 degrees C/min and calcination temperature at 500 degrees C for 2 h, the optimized alpha-Fe2O3 nanotubes are obtained. These alpha-Fe2O3 nanotubes have a magnetization (M-s) of 0.36 emu . g(-1) and coercivity (H-c) of 1942 Oe and can be used in the nanospace technology.
引用
收藏
页码:2670 / 2673
页数:4
相关论文
共 21 条
[11]   Electrospinning: A simple and versatile technique for producing ceramic nanofibers and nanotubes [J].
Li, Dan ;
McCann, Jesse T. ;
Xia, Younan .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2006, 89 (06) :1861-1869
[12]   Surfactant-assisted synthesis of α-Fe2O3 nanotubes and nanorods with shape-dependent magnetic properties [J].
Liu, Lu ;
Kou, Hui-Zhong ;
Mo, Wenling ;
Liu, Huajie ;
Wang, Yuqiu .
JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (31) :15218-15223
[13]   Smart nanotubes for bioseparations and biocatalysis [J].
Mitchell, DT ;
Lee, SB ;
Trofin, L ;
Li, NC ;
Nevanen, TK ;
Söderlund, H ;
Martin, CR .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2002, 124 (40) :11864-11865
[14]   In situ generated dense shell-engaged Ostwald ripening: A facile controlled-preparation for BaFe12O19 hierarchical hollow fiber arrays [J].
Mou, Fang-zhi ;
Guan, Jian-guo ;
Sun, Zhi-gang ;
Fan, Xi-an ;
Tong, Guo-xiu .
JOURNAL OF SOLID STATE CHEMISTRY, 2010, 183 (03) :736-743
[15]   Magnetic nanotubes for magnetic-field-assisted bioseparation, biointeraction, and drug delivery [J].
Son, SJ ;
Reichel, J ;
He, B ;
Schuchman, M ;
Lee, SB .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2005, 127 (20) :7316-7317
[16]   Magnetic-field-induced growth of single-crystalline Fe3O4 nanowires [J].
Wang, J ;
Chen, QW ;
Zeng, C ;
Hou, BY .
ADVANCED MATERIALS, 2004, 16 (02) :137-+
[17]   Fabrication and characterization of Fe-Ni alloy/nickel ferrite composite nanofibers by electrospinning and partial reduction [J].
Xiang, Jun ;
Shen, Xiangqian ;
Song, Fuzhan ;
Liu, Mingquan ;
Zhou, Guangzhen ;
Chu, Yanqiu .
MATERIALS RESEARCH BULLETIN, 2011, 46 (02) :258-261
[18]   Mesoporous metal-organic framework materials [J].
Xuan, Weimin ;
Zhu, Chengfeng ;
Liu, Yan ;
Cui, Yong .
CHEMICAL SOCIETY REVIEWS, 2012, 41 (05) :1677-1695
[19]   Facile fabrication of long α-Fe2O3, α-Fe and γ-Fe2O3 hollow fibers using sol-gel combined co-elecrospinning technology [J].
Zhan, Sihui ;
Chen, Dairong ;
Jiao, Xiuling ;
Liu, Shusheng .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2007, 308 (01) :265-270
[20]   Highly Ordered TiO2 Nanotube Arrays: Recent Advances in Fabrication and Environmental Applications-A Review [J].
Zhang, Qian ;
Xu, Hao ;
Yan, Wei .
NANOSCIENCE AND NANOTECHNOLOGY LETTERS, 2012, 4 (05) :505-519