Synthesis of oximes under ultrasound irradiation

被引：69

作者：

Li, JT ^{[1
]}

Li, XL ^{[1
]}

Li, TS ^{[1
]}

机构：

[1] Hebei Univ, Coll Chem & Environm Sci, Key Lab Analyt Sci & Technol Hebei Province, Baoding 071002, Peoples R China

来源：

ULTRASONICS SONOCHEMISTRY | 2006年 / 13卷 / 03期

关键词：

condensation; oxime; ultrasound;

D O I：

10.1016/j.ultsonch.2005.11.011

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

The condensation of aldehydes and ketones with hydroxylamine hydrochloride results oximes in 50.7-98.7% yields in EtOH under ultrasound irradiation. Compared with conventional methods, the main advantages of the present procedure are milder conditions, shorter reaction time and higher yields. (c) 2005 Elsevier B.V. All rights reserved.

引用

页码：200 / 202

页数：3

共 22 条

[1]

BROWN NC, 1964, Patent No. 960241

[2] CHLORINATION OF OXIMES .1. REACTION AND MECHANISM OF CHLORINATION OF OXIMES IN COMMERCIAL CHLOROFORM AND METHYLENE CHLORIDE [J].