Synthesis and Crystal Structures of Complexes of Copper, Silver Assembled by Diniconazole

被引：0

作者：

Nie Xu-Liang ^{[1
]}

Xiong Hui ^{[1
]}

Tu Yong-Gang ^{[2
]}

Huang Chang-Gan ^{[1
]}

机构：

[1] Jiangxi Agr Univ, Coll Sci, Nanchang 330045, Peoples R China

[2] Jiangxi Agr Univ, Coll Food Sci & Engn, Nanchang 330045, Peoples R China

来源：

CHINESE JOURNAL OF INORGANIC CHEMISTRY | 2012年 / 28卷 / 12期

关键词：

copper complex; silver complex; diniconazole; hydrothermal synthesis; crystal structure;

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two new complexes [CuL4Cl2] (1) and [AgL2]NO3 (2) (L=diniconazole) were synthesized by solvothermal condition and structurally characterized by element analysis, IR and single crystal X-ray diffraction. Complex 1 is the Triclinic system, space group P (1) over bar with a=0.882 3(7) nm, b=1.370 5(10) nm, c=1.516 4(11) nm, alpha=91.507(11)degrees, beta=97.356(9)degrees, gamma=107.683(9)degrees. Complex 2 belongs to the Monoclinic system, space group P2(1)/c with a=1.229 2(3) nm, b=1.272 1(3) nm, c=2.431 7(5) nm, alpha=90 degrees, beta=98.694(3)degrees, gamma=90 degrees. 1 and 2 are linked into a one dimensional chain by intermolecular hydrogen bonds. CCDC: 805738, 1; 818240, 2.

引用

页码：2593 / 2596

页数：4

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