On the impact of nanometric ?' precipitates on the tensile deformation of superelastic Co49Ni21Ga30

被引:3
作者
Reul, A. [1 ]
Lauhoff, C. [2 ]
Krooss, P. [2 ]
Somsen, C. [3 ]
Langenkaemper, D. [3 ]
Gutmann, M. J. [4 ]
Pedersen, B. [5 ]
Hofmann, M. [5 ]
Gan, W. M. [6 ]
Kireeva, I. [7 ]
Chumlyakov, Y. I. [7 ]
Eggeler, G. [3 ]
Niendorf, T. [2 ]
Schmahl, W. W. [1 ]
机构
[1] Ludwig Maximilian Univ Munich, Dept Earth & Environm Sci, Appl Crystallog, D-80333 Munich, Germany
[2] Univ Kassel, Inst Mat Engn, D-34125 Kassel, Germany
[3] Ruhr Univ Bochum, Inst Mat, D-44801 Bochum, Germany
[4] Rutherford Appleton Lab, ISIS Facil, Didcot OX11 0QX, Oxon, England
[5] Tech Univ Munich, Heinz Maier Leibnitz Zentrum MLZ, D-85748 Garching, Germany
[6] Helmholtz Zentrum Hereon, German Engn Mat Sci Ctr GEM MLZ, D-85748 Garching, Germany
[7] Tomsk State Univ, Siberian Phys Tech Inst, Novosobornay Sq 1, Tomsk 634050, Russia
关键词
Martensitic transformation; Microstructure; Neutron diffraction; Single crystals; Superelasticity; SHAPE-MEMORY ALLOY; CO-NI-GA; SINGLE-CRYSTALS; MARTENSITIC-TRANSFORMATION; PHASE-TRANSFORMATIONS; COMPRESSION ASYMMETRY; CYCLIC DEFORMATION; MICROSTRUCTURE; PSEUDOELASTICITY; MECHANISMS;
D O I
10.1016/j.actamat.2022.117835
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Results are presented reporting on the martensite domain variant selection and stress-induced martensite morphology in [001]-oriented superelastic Co49Ni21Ga30 shape memory alloy (SMA) single crystals under tensile load. In situ neutron diffraction, as well as in situ optical-and confocal laser scanning microscopy were conducted focusing on three differently treated samples, i.e. in the as-grown, solution-annealed and aged condition. An aging treatment performed at 350 ? promotes the precipitation of nanoprecipitates. These second phase precipitates contribute to an increase of the number of habit plane interfaces, while reducing lamellar martensite plate thickness compared to the as-grown and solution-annealed (precipitate free) samples. During tensile loading, all samples show a stress-induced formation of martensite, characterized by one single domain variant ( "detwinned ") and one set of parallel habit planes in a shear band. The results clearly show that gamma' nanoprecipitates do not necessarily promote multi-variant interaction during tensile loading. Thus, reduced recoverability in Co-Ni-Ga SMAs upon aging cannot be solely attributed to this kind of interaction as has been proposed in literature so far.& nbsp;(C) 2022 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
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页数:11
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