Synthesis of 13C-labelled tetramethyltetraselenafulvalene

被引：3
作者：
Christensen, JB
Bechgaard, K
Paquignon, G
机构：
[1] Univ Copenhagen, Dept Chem, Mat Sci Lab, DK-2100 Copenhagen, Denmark
[2] Riso Natl Lab, Condensed Matter Phys & Chem Dept, DK-4000 Roskilde, Denmark
[3] CEA, CENG, LCP, SPSMS,DRFMC, F-38054 Grenoble, France
来源：
JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS | 2001年 / 44卷 / 14期
关键词：
heterocyclic selenium compounds; organic superconductors; C-13-labelling; carbondiselenide; TMTSF; 4,5-dimethyl-1,3-diselenole-2-selone;
D O I：
10.1002/jlcr.525
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
The synthesis of tetramethyltetraselenafulvalene (4,4',5,5'-tetramethyl Delta (2,2')-bis-1,3-diselenole) doubly labelled with carbon-13 in the 2 and 2'-positions is described. Copyright (C) 2001 John Wiley & Sons, Ltd.
引用
收藏
页码：1035 / 1041
页数：7
相关论文
共 16 条
  • [1] NMR IN COMMENSURATE AND INCOMMENSURATE SPIN-DENSITY WAVES
    BARTHEL, E
    QUIRION, G
    WZIETEK, P
    JEROME, D
    CHRISTENSEN, JB
    JORGENSEN, M
    BECHGAARD, K
    [J]. EUROPHYSICS LETTERS, 1993, 21 (01): : 87 - 92
  • [2] C-13 NMR INVESTIGATION OF THE LINEAR AND NONLINEAR DYNAMICS OF THE SPIN-DENSITY-WAVE OF (TMTSF)2PF6
    BARTHEL, E
    KRIZA, G
    QUIRION, G
    WZIETEK, P
    JEROME, D
    CHRISTENSEN, JB
    JORGENSEN, M
    BECHGAARD, K
    [J]. JOURNAL DE PHYSIQUE IV, 1993, 3 (C2): : 231 - 234
  • [3] MOTIONAL NARROWING OF THE NUCLEAR-MAGNETIC-RESONANCE LINE BY THE SLIDING OF SPIN-DENSITY WAVES
    BARTHEL, E
    QUIRION, G
    WZIETEK, P
    JEROME, D
    CHRISTENSEN, JB
    JORGENSEN, M
    BECHGAARD, K
    [J]. JOURNAL DE PHYSIQUE I, 1993, 3 (07): : 1501 - 1505
  • [4] CONDUCTION NOISE AND MOTIONAL NARROWING OF THE NUCLEAR-MAGNETIC-RESONANCE LINE IN SLIDING SPIN-DENSITY WAVES
    BARTHEL, E
    KRIZA, G
    QUIRION, G
    WZIETEK, P
    JEROME, D
    CHRISTENSEN, JB
    JORGENSEN, M
    BECHGAARD, K
    [J]. PHYSICAL REVIEW LETTERS, 1993, 71 (17) : 2825 - 2828
  • [5] BARTHEL E, 1993, SYNTHETIC MET, V55, P2581
  • [6] SUPERCONDUCTIVITY IN AN ORGANIC-SOLID - SYNTHESIS, STRUCTURE, AND CONDUCTIVITY OF BIS(TETRAMETHYLTETRASELENAFULVALENIUM) PERCHLORATE, (TMTSF)2CLO4
    BECHGAARD, K
    CARNEIRO, K
    RASMUSSEN, FB
    OLSEN, M
    RINDORF, G
    JACOBSEN, CS
    PEDERSEN, HJ
    SCOTT, JC
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1981, 103 (09) : 2440 - 2442
  • [7] SYNTHESIS OF 1,3-DISELENOLE-2-SELONES AND 1,3-DISELENOLE-2-THIONES
    BECHGAARD, K
    COWAN, DO
    BLOCH, AN
    HENRIKSEN, L
    [J]. JOURNAL OF ORGANIC CHEMISTRY, 1975, 40 (06) : 746 - 749
  • [8] MOLECULAR QUADRUPOLE-MOMENT AND MAGNETIC-ANISOTROPY OF CARBON DISELENIDE
    BRERETON, MP
    COOPER, MK
    DENNIS, GR
    RITCHIE, GLD
    [J]. AUSTRALIAN JOURNAL OF CHEMISTRY, 1981, 34 (11) : 2253 - 2261
  • [9] Charge ordering in the TMTTF family of molecular conductors
    Chow, DS
    Zamborszky, E
    Alavi, B
    Tantillo, DJ
    Baur, A
    Merlic, CA
    Brown, SE
    [J]. PHYSICAL REVIEW LETTERS, 2000, 85 (08) : 1698 - 1701
  • [10] CHRISTENSEN JJ, UNPUB
12