Powders: chemical preparatiom;
Composite;
Chemical properties Heterogeneous nucleation processing;
HETEROGENEOUS NUCLEATION;
MICROSTRUCTURE;
COMPOSITE;
MONAZITE;
BEHAVIOR;
ALUMINA;
GROWTH;
D O I:
10.1016/j.ceramint.2008.03.014
中图分类号:
TQ174 [陶瓷工业];
TB3 [工程材料学];
学科分类号:
0805 ;
080502 ;
摘要:
LaPO4-coated alpha-Al2O3 powders were successfully synthesized through the heterogeneous precipitation method. The coated powders were characterized by XRD, TEM. EDS, and zeta-potential measurements. According to the XRD results, the coated powders consisted of only alpha-Al2O3 and monoclinic LaPO4. The TEM examinations and EDS analysis showed that under alkaline condition a homogeneous coating with thickness of similar to 10 nm was obtained on the alpha-Al2O3 powder surface. The zeta-potential measurements showed the coated powders to have a pH value of 7.85 at isoelectric point, similar to that of LaPO4 (pH value of 8.21). This was in good agreement with the TEM and EDS results, indicating a successful coating process in our experiment. (C) 2008 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
机构:
Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R ChinaChinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China
Lu, JS
Gao, L
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Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R ChinaChinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China
Gao, L
Gui, LH
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机构:
Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R ChinaChinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China
Gui, LH
Guo, JK
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机构:
Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R ChinaChinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China
Department of Ceramic Engineering, National Institute of Technology, Rourkela
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机构:
Department of Ceramic Engineering, National Institute of Technology, RourkelaDepartment of Ceramic Engineering, National Institute of Technology, Rourkela
Department of Ceramic Engineering, National Institute of Technology, Rourkela
769008, India
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机构:Department of Ceramic Engineering, National Institute of Technology, Rourkela
机构:
Canakkale Onsekiz Mart Univ, Can Vocat Sch, Dept Mat & Mat Proc Technol, TR-17400 Canakkale, TurkeyCanakkale Onsekiz Mart Univ, Can Vocat Sch, Dept Mat & Mat Proc Technol, TR-17400 Canakkale, Turkey
Abali, Serkan
Ekerim, Ahmet
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机构:
Yildiz Tech Univ, Fac Chem & Met Engn, Dept Met & Mat, TR-34210 Istanbul, TurkeyCanakkale Onsekiz Mart Univ, Can Vocat Sch, Dept Mat & Mat Proc Technol, TR-17400 Canakkale, Turkey