A Novel One-Pot Synthesis of UV-Blue ZnSe Nanocrystals in Aqueous Solution

被引：1
|
作者：
Fu, Shasha [1 ]
Sun, Qizhuang [1 ]
Li, Dingyun [1 ]
Dong, Meiting [1 ]
Liu, Shuxian [1 ]
Huang, Chaobiao [1 ]
机构：
[1] Zhejiang Normal Univ, Coll Chem & Life Sci, Jinhua 321004, Zhejiang, Peoples R China
来源：
JOURNAL OF THE CHINESE CHEMICAL SOCIETY | 2013年 / 60卷 / 03期
关键词：
One-pot; Aqueous solution; ZnSe quantum dots; MICROWAVE ENZYMATIC DIGESTION; ALLOYED QUANTUM DOTS; HYDROTHERMAL SYNTHESIS; CDTE NANOCRYSTALS; CDSE NANOCRYSTALS; REVERSE MICELLE; SHAPE CONTROL; CAPPED ZNSE; GLUTATHIONE; CORE/SHELL;
D O I：
10.1002/jccs.201200204
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Described herein is a novel one-pot aqueous synthesis of ZnSe nanocrystals has featuring the utilization of Na2SeO3 and Zn(AC)(2)center dot 2H(2)O as Se and Zn source, glutathione (GSH) as stabilizing agent and reducing agent. By this approach, the UV-blue ZnSe QDs with quantum yield (QYs) up to 19% have been synthesized with a molar ratio of Se/Zn/GSH at 1:4:8.5 under aqueous conditions at 110 degrees C. XRD and TEM show the ZnSe QDs are zinc cubic structure particles with an average diameter of 3-5 nm.
引用
收藏
页码：309 / 313
页数：5
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