Novel satellites in a two-dimensional spin-echo NMR experiment for homonuclear dipole-coupled spins in rotating solids

被引：3

作者：

Kuwahara, D ^{[1
]}

Nakai, T

Ashida, J

Miyajima, S

机构：

[1] Inst Mol Sci, Okazaki, Aichi 4448585, Japan

[2] Tokyo Univ Agr & Technol, Koganei, Tokyo 1848588, Japan

[3] Kyoto Univ, Fac Sci, Dept Chem, Kyoto 6068224, Japan

来源：

CHEMICAL PHYSICS LETTERS | 1999年 / 305卷 / 1-2期

关键词：

D O I：

10.1016/S0009-2614(99)00356-5

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Additional resonance lines emerged along the F-1 axis on a two-dimensional (2D) NMR spectrum, when the 2D spin-echo pulse sequence was applied to a solid-state homonuclear two-spin system with a negligibly small J-coupling constant under magic-angle sample spinning. We found that the positions of the lines are determined by the sample spinning frequency and the difference of the isotropic chemical shifts. (C) 1999 Elsevier Science B.V. All rights reserved.

引用

页码：35 / 38

页数：4

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