Superparamagnetic behavior of nanosized ZnFe2O4

被引:14
作者
Dey, S. [1 ]
Mondal, R. [1 ]
Majumder, S. [1 ,2 ]
Dasgupta, P. [2 ]
Poddar, A. [2 ]
Banerjee, S. [2 ]
Kumar, S. [1 ]
机构
[1] Jadavpur Univ, Dept Phys, Kolkata 700032, India
[2] Saha Inst Nucl Phys, 1-AF Bidhannagar, Kolkata 700064, India
关键词
Ferrite; Rietveld refinement; Mossbauer spectroscopy; dc magnetic study; ZINC FERRITE NANOPARTICLES; MAGNETIC-PROPERTIES; COPRECIPITATION METHOD; ENHANCEMENT;
D O I
10.1016/j.matpr.2017.10.177
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Herein, we have reported the structural, microstructural, magnetic and hyperfine properties of nanosized (similar to 20 nm) ZnFe2O4 synthesized by flow rate controlled coprecipitation method. The PXRD and HRTEM study demonstrate that the sample is nanosized, single phase spinel oxide which crystallizes in Fd (3) over barm space group. The sample exhibits superparamagnetic relaxation above blocking temperature (similar to 25 K). The saturation magnetizations of the sample are 4, 20 and 28 emu g(-1) at 300, 100 and 10 K, respectively and the sample exhibits no hysteresis at 300 and 100 K. (C) 2017 Elsevier Ltd. All rights reserved. Selection and/or Peer-review under responsibility of International Conference on Functional Nano-Materials, 2016.
引用
收藏
页码:9855 / 9859
页数:5
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