Ion chromatography determination of chloride and sulphate in cement

被引:14
作者
Poznic, M [1 ]
Gabrovsek, R [1 ]
Novic, M [1 ]
机构
[1] Natl Inst Chem, Ljubljana 1001, Slovenia
关键词
chloride; sulfate; characterization; cement;
D O I
10.1016/S0008-8846(98)00234-8
中图分类号
TU [建筑科学];
学科分类号
0813 ;
摘要
The contents of chlorine and sulphur species in commercial portland cement were determined by a two-step sample preparation procedure. The first step was carried out by means of sodium carbonate and peroxide fusion, followed by a second step of electrodialytic neutralisation of the resulting solution. The chloride and sulphate contents were then determined by ion chromatography. The accuracy of the method was checked by analysing a certified standard reference material (SRM). Relative standard deviations were 0.56% and 1.35% for sulphur and chloride determination, respectively. (C) 1999 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:441 / 443
页数:3
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