Electrochemical Synthesis of 2-Amino-5-(2-methylphenyl)-1,3,4-oxadiazoles

被引：3
作者：
Kumar, Sanjeev [1 ]
机构：
[1] Univ Allahabad, Iswar Saran Degree Coll, Dept Chem, Allahabad 211004, Uttar Pradesh, India
来源：
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES INDIA SECTION A-PHYSICAL SCIENCES | 2012年 / 82卷 / 02期
关键词：
Synthesis; 2-Amino-5-(2-methylphenyl)-1,3,4-oxadiazole; Electrooxidation; Controlled potential electrolysis; ANTIINFLAMMATORY ACTIVITY; 1,3,4-OXADIAZOLES; ANTIBACTERIAL; ALDEHYDES; SERIES;
D O I：
10.1007/s40010-012-0028-6
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
2-Amino-5-(2-methylphenyl)-1,3,4-oxadiazole derivatives were synthesized by electrochemical oxidation of semicarbazone at platinum electrode. The resulting compounds were characterized by elemental analyses, IR, H-1 and C-13 NMR spectral data. The electrolysis was carried out in acetonitrile using lithium perchlorate as a supporting electrolyte. Two platinum plates were used as working as well as counter electrode and saturated calomel electrode as a reference electrode.
引用
收藏
页码：157 / 162
页数：6
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