Microwave hydrothermal synthesis of nanosize Ta2O5 added Mg-Cu-Zn ferrites

被引:27
作者
Krishnaveni, T [1 ]
Murthy, SR
Gao, F
Lu, Q
Komarneni, S
机构
[1] Osmania Univ, Dept Phys, Hyderabad 500007, Andhra Pradesh, India
[2] Penn State Univ, Mat Res Inst, University Pk, PA 16802 USA
基金
美国国家科学基金会;
关键词
D O I
10.1007/s10853-006-7488-5
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Tantalum oxide added MgCuZn ferrite powders were synthesized by a co-precipitation method using NaOH in a microwave-hydrothermal (M-H) apparatus. The phase identification of the prepared samples was done by X-ray diffraction and crystal size and morphology were determined by transmission electron microscopy (TEM). Nano-phase ferrites with high surface area were synthesized at 160 degrees C after a treatment time of 1 hour. The M-H synthesized powders were conventionally sintered at a temperature of 900 degrees C/4h. The variations of the sintered density, initial permeability and electrical resistivity as a function of additive concentration at room temperature have been investigated. (c) 2006 Springer Science + Business Media, Inc.
引用
收藏
页码:1471 / 1474
页数:4
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