Spectrophotometric determination of hydrogen peroxide with osmium(VIII) and m-carboxyphenylfluorone

被引:43
作者
Hoshino, Mitsuru [1 ]
Kamino, Shinichiro [1 ]
Doi, Mitsunobu [1 ]
Takada, Shingo [1 ]
Mitani, Shota [1 ]
Yanagihara, Rika [1 ]
Asano, Mamiko [1 ]
Yamaguchi, Takako [1 ]
Fujita, Yoshikazu [1 ]
机构
[1] Osaka Univ Pharmaceut Sci, Takatsuki, Osaka 5691094, Japan
关键词
Spectrophotometry; Hydrogen peroxide; Osmium(VIII); m-Carboxyphenylfluorone; Colored complex; SENSITIVITY;
D O I
10.1016/j.saa.2013.08.048
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
Spectrophotometric determination of hydrogen peroxide was accomplished with osmium(VIII) and m-carboxyphenylfluorone (MCPF) in the presence of cetyltrimethylammonium chloride (CTAC). In the determination of hydrogen peroxide based on the fading of the color of osmium(VIII)-MCPF complex, Beer's law was obeyed in the range 20-406 ng mL(-1), with an effective molar absorption coefficient (at 580 nm) of 5.21. x 10(4) L mol(-1) cm(-1) and a relative standard deviation of 0.33% (n = 6). Further, we performed the characterization of MCPF and obtained the crystal structure. (C) 2013 Elsevier B.V. All rights reserved.
引用
收藏
页码:814 / 816
页数:3
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