Process stabilization during reactive high power impulse magnetron sputtering of Ce/Gd target

被引:2
作者
Rabotkin, S. V. [1 ]
Oskirko, V. O. [1 ]
Ionov, I. V. [1 ]
Semenov, V. A. [1 ]
Shipilova, A. V. [1 ]
Solovyev, A. A. [1 ]
机构
[1] RAS, Inst High Current Elect SB, 2-3 Akademichesky Ave, Tomsk 634055, Russia
来源
6TH INTERNATIONAL CONGRESS ENERGY FLUXES AND RADIATION EFFECTS | 2018年 / 1115卷
基金
俄罗斯科学基金会;
关键词
THIN-FILMS; DEPOSITION; DENSE; VOLTAGE; ZRO2;
D O I
10.1088/1742-6596/1115/3/032078
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
In this study, a simple approach to stabilize reactive high power impulse magnetron sputtering process in the transition zone between the metallic and oxide modes was investigated. The method is based on the use of peak current value as feedback and control signal. It was shown that the change in the state of the target surface causes almost instantaneous change in the amplitude and shape of the current pulses. To stabilize the deposition process, the pulse frequency was regulated to maintain a constant maximum discharge current. The hysteresis behavior and the variations of the pulse current waveforms over a wide range of O-2 flow rates and pulse frequencies during a reactive HiPIMS deposition of gadolinia-doped ceria (GDC) thin films in an Ar-O-2 atmosphere were examined. Stable process conditions were maintained at the O-2 flow from 0.9 to 3.9 sccm by adjustment of the pulse frequency from 1.45 to 2.9 kHz. GDC films deposited using peak current regulation exhibited a stable stoichiometry and high deposition rate in comparison with films obtained without process stabilization.
引用
收藏
页数:7
相关论文
共 20 条
  • [1] MECHANISMS OF VOLTAGE-CONTROLLED, REACTIVE, PLANAR MAGNETRON SPUTTERING OF AL IN AR-N2 AND AR-O2 ATMOSPHERES
    AFFINITO, J
    PARSONS, RR
    [J]. JOURNAL OF VACUUM SCIENCE & TECHNOLOGY A, 1984, 2 (03): : 1275 - 1284
  • [2] Understanding the discharge current behavior in reactive high power impulse magnetron sputtering of oxides
    Aiempanakit, Montri
    Aijaz, Asim
    Lundin, Daniel
    Helmersson, Ulf
    Kubart, Tomas
    [J]. JOURNAL OF APPLIED PHYSICS, 2013, 113 (13)
  • [3] The role of the erosion groove during reactive sputter deposition
    Depla, D.
    Strijckmans, K.
    De Gryse, R.
    [J]. SURFACE & COATINGS TECHNOLOGY, 2014, 258 : 1011 - 1015
  • [4] Magnetron sputter deposition: Linking discharge voltage with target properties
    Depla, D.
    Mahieu, S.
    De Gryse, R.
    [J]. THIN SOLID FILMS, 2009, 517 (09) : 2825 - 2839
  • [5] CrN thin films deposited by HiPIMS in DOMS mode
    Ferreira, F.
    Oliveira, J. C.
    Cavaleiro, A.
    [J]. SURFACE & COATINGS TECHNOLOGY, 2016, 291 : 365 - 375
  • [6] Titanium oxide thin films deposited by high-power impulse magnetron sputtering
    Konstantinidis, S.
    Dauchot, J. P.
    Hecq, A.
    [J]. THIN SOLID FILMS, 2006, 515 (03) : 1182 - 1186
  • [7] A novel pulsed magnetron sputter technique utilizing very high target power densities
    Kouznetsov, V
    Macák, K
    Schneider, JM
    Helmersson, U
    Petrov, I
    [J]. SURFACE & COATINGS TECHNOLOGY, 1999, 122 (2-3) : 290 - 293
  • [8] Fully dense, non-faceted 111-textured high power impulse magnetron sputtering TiN films grown in the absence of substrate heating and bias
    Lattemann, M.
    Helmersson, U.
    Greene, J. E.
    [J]. THIN SOLID FILMS, 2010, 518 (21) : 5978 - 5980
  • [9] REACTIVE DEPOSITION OF HARD COATINGS
    MUSIL, J
    KADLEC, S
    VYSKOCIL, J
    POULEK, V
    [J]. SURFACE & COATINGS TECHNOLOGY, 1989, 39 (1-3) : 301 - 314
  • [10] Dense yttria-stabilised zirconia electrolyte layers for SOFC by reactive magnetron sputtering
    Nedelec, R.
    Uhlenbruck, S.
    Sebold, D.
    Haanappel, V. A. C.
    Buchkremer, H-P
    Stoever, D.
    [J]. JOURNAL OF POWER SOURCES, 2012, 205 : 157 - 163