Sample-preparation methods for pesticide-residue analysis in cereals and derivatives

被引：66

作者：

Angel Gonzalez-Curbelo, Miguel ^{[1
]}

Herrera-Herrera, Antonio V. ^{[1
]}

Ravelo-Perez, Lidia M. ^{[1
]}

Hernandez-Borges, Javier ^{[1
]}

机构：

[1] ULL, Fac Quim, Dept Quim Analit Nutr & Bromatol, San Cristobal la Laguna 38206, Tenerife, Spain

来源：

TRAC-TRENDS IN ANALYTICAL CHEMISTRY | 2012年 / 38卷

关键词：

Analytical method; Baby food; Cereal; Flour; Food safety; Pesticide; Pesticide derivative; Pesticide-residue analysis (PRA); Sample preparation; Sample pretreatment; TANDEM MASS-SPECTROMETRY; PERFORMANCE LIQUID-CHROMATOGRAPHY; SOLID-PHASE EXTRACTION; ACCELERATED SOLVENT-EXTRACTION; ELECTRON-CAPTURE DETECTION; EASY MULTIRESIDUE METHOD; RICE ORYZA-SATIVA; GAS-CHROMATOGRAPHY; HERBICIDE RESIDUES; MICROEXTRACTION FIBER;

D O I：

10.1016/j.trac.2012.04.010

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Since the Neolithic Age, cereals have constituted an important part of the human diet, and they are now one of the foods most produced and consumed in the world. As a result, and because of the large population involved, food-safety issues are an important matter of concern and appropriate action is required. Pesticide-residue analysis, including method optimization, method development and monitoring programs are becoming increasingly important. The aim of this review article is to provide a general overview of the different sample-preparation methods published in the period 2006-11 covering the analysis of pesticides in cereal samples, including some of their derivatives, such as flour or cereal-based baby foods. (c) 2012 Elsevier Ltd. All rights reserved.

引用

页码：32 / 51

页数：20

共 60 条

[1] Simplified determination of combined residues of lindane and other HCH isomers in vegetables, fruits, wheat, pulses and medicinal plants by matrix solid-phase dispersion (MSPD) followed by GC-ECD [J].

Abhilash, P. C. ;

Singh, Vandana ;

Singh, Nandita .

FOOD CHEMISTRY, 2009, 113 (01) :267-271

[2] Evaluation of supercritical fluid extraction/aminopropyl solid-phase "in-line" cleanup for analysis of pesticide residues in rice [J].

Aguilera, A ;

Rodríguez, M ;

Brotons, M ;

Boulaid, M ;

Valverde, A .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2005, 53 (24) :9374-9382

[3]

Anastassiades M, 2003, J AOAC INT, V86, P412

[4] Solid-phase extraction on sorbents of different retention mechanisms followed by determination by gas chromatography-mass spectrometric and gas chromatography-electron capture detection of pesticide residues in crops [J].

Balinova, Anna ;

Mladenova, Rositsa ;

Shtereva, Deyana .

JOURNAL OF CHROMATOGRAPHY A, 2007, 1150 (1-2) :136-144

[5]

Bar-L'Helgouac'h C., 2004, Quality control of cereals and pulses: practical guide

[6]

Boccacci Mariani M., 2010, Journal of AOAC International, V93, P999

[7] Determination of benzoylurea insecticides in food by pressurized liquid extraction and LC-MS [J].

Brutti, Monia ;

Blasco, Cristina ;

Pico, Yolanda .

JOURNAL OF SEPARATION SCIENCE, 2010, 33 (01) :1-10

[8] Sensitive determination of herbicides in food samples by nonaqueous CE using pressurized liquid extraction [J].

Carabias-Martinez, Rita ;

Rodriguez-Gonzalo, Encarnacion ;

Miranda-Cruz, Edith ;

Dominguez-Alvarez, Javier ;

Hernandez-Mendez, Jesus .

ELECTROPHORESIS, 2007, 28 (20) :3606-3616

[9] Organophosphorus pesticide residues in milled rice (Oryza sativa) on the Chinese market and dietary risk assessment [J].

Chen, Chen ;

Li, Yun ;

Chen, Mingxue ;

Chen, Zhijun ;

Qian, Yongzhong .

FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 2009, 26 (03) :340-347

[10] Cloud point extraction coupled with derivative of carbofuran as a preconcentration step prior to HPLC [J].

Chen, Jian-bo ;

Zhao, Wei-jun ;

Liu, Wei ;

Zhou, Zhi-ming ;

Yang, Ming-min .

FOOD CHEMISTRY, 2009, 115 (03) :1038-1041

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