N-(3-chlorophenyl)benzenesulfonamide

被引：12

作者：

Gowda, B. Thimme ^{[1
]}

Foro, Sabine ^{[2
]}

Babitha, K. S. ^{[1
]}

Fuess, Hartmut ^{[2
]}

机构：

[1] Mangalore Univ, Dept Chem, Mangalore 574199, India

[2] Tech Univ Darmstadt, Inst Mat Sci, D-64287 Darmstadt, Germany

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷

关键词：

D O I：

10.1107/S1600536808026895

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the crystal structure of the title compound, C(12)H(10)ClNO(2)S, the N-H bond is trans to one of the S = O bonds. The two aromatic rings form a dihedral angle of 65.4 (1)degrees, compared with a value of 49.1 (1)degrees in N-(2-chlorophenyl)-benzenesulfonamide. The molecules are connected by intermolecular N-H center dot center dot center dot O hydrogen bonds into chains running along the b axis.

引用

页码：O1825 / U2547

页数：9

共 11 条

[1]

*ENR NON, 1996, CAD 4 PC

[2] ON ENANTIOMORPH-POLARITY ESTIMATION [J].

FLACK, HD .

ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (NOV) :876-881

[3] Structural systematics of 4,4′-disubstituted benzenesulfonamidobenzenes.: 1.: Overview and dimerbased isostructures [J].

Gelbrich, Thomas ;

Hursthouse, Michael B. ;

Threlfall, Terence L. .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 2007, 63 (04) :621-632

[4] N-(2-methylphenyl)benzenesulfonamide [J].

Gowda, B. Thimme ;

Foro, Sabine ;

Babitha, K. S. ;

Fuess, Hartmut .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 :O1692-U1364

[5] N-(2,6-dimethylphenyl)benzenesulfonamide [J].

Gowda, B. Thimme ;

Foro, Sabine ;

Babitha, K. S. ;

Fuess, Hartmut .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 :O1691-U1354

[6] Synthetic, infrared, 1H and 13C NMR spectral studies on N-(2-/3-substituted phenyl)-4-substituted benzenesulphonamides, 4-X′C6H4SO2NH(2-/3-XC6H4)1 where X′ = H, CH3, C2H5, F, Cl or Br, and X = CH3 or Cl [J].

Gowda, BT ;

Shetty, M ;

Jayalakshmi, KL .

ZEITSCHRIFT FUR NATURFORSCHUNG SECTION A-A JOURNAL OF PHYSICAL SCIENCES, 2005, 60 (1-2) :106-112

[7] A SEMI-EMPIRICAL METHOD OF ABSORPTION CORRECTION [J].

NORTH, ACT ;

PHILLIPS, DC ;

MATHEWS, FS .

ACTA CRYSTALLOGRAPHICA SECTION A-CRYSTAL PHYSICS DIFFRACTION THEORETICAL AND GENERAL CRYSTALLOGRAPHY, 1968, A 24 :351-&

[8] N-(2-chlorophenyl)benzenesulfonamide [J].

Perlovich, GL ;

Tkachev, VV ;

Schaper, KJ ;

Raevsky, OA .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 :O780-O782

[9] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[10] Single-crystal structure validation with the program PLATON [J].

Spek, AL .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13

← 1 2 →