Synthesis and characterization of crystalline hexagonal bipods of zinc oxide

被引：85
作者：
Bitenc, Marko [1 ]
Orel, Zorica Crnjak [1 ]
机构：
[1] Natl Inst Chem, SI-1000 Ljubljana, Slovenia
来源：
MATERIALS RESEARCH BULLETIN | 2009年 / 44卷 / 02期
关键词：
Nanostructures; Semiconductor; Chemical synthesis; Electron microscopy; Infrared spectroscopy; ZNO NANOSTRUCTURES; LOW-TEMPERATURE; CONTROLLABLE SYNTHESIS; NANOSIZE PRECURSORS; GROWTH-MECHANISM; PARTICLES; ROUTE; NANOCRYSTALS; AGGREGATION; NANOWIRES;
D O I：
10.1016/j.materresbull.2008.05.005
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
The preparation of nano- and submicrometre-sized one-dimensional (1D) zinc oxides (ZnOs) from zinc nitrate was performed by precipitation with urea in two types of solvents (water and water/polyol mixtures). The influence of different polyols (ethylene glycol, diethylene glycol and tetraethylene glycol) on the size of the final particles (length and diameter) is presented for the first time. As well as the influence of the solvents used, the ratio of water/polyol, temperature, pH and time of synthesis was correlated with the size and morphology of the final particles. In all cases crystalline ZnO was synthesized in the form of hexagonal bipods. The morphological and crystalline properties of the samples obtained were characterized by SEM, IR, and XRD. (C) 2008 Elsevier Ltd. All rights reserved.
引用
收藏
页码：381 / 387
页数：7
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