2-Aminoterephthalic acid dimethyl ester

被引:5
作者
Bruening, Juergen [1 ]
Bats, Jan W. [2 ]
Schmidt, Martin U. [1 ]
机构
[1] Goethe Univ Frankfurt, Inst Inorgan & Analyt Chem, D-60438 Frankfurt, Germany
[2] Goethe Univ Frankfurt, Inst Organ Chem & Chem Biol, D-60438 Frankfurt, Germany
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词
D O I
10.1107/S1600536809036095
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Single crystals of the title compound, C10H11NO4, an intermediate in the industrial synthesis of yellow azo pigments, were obtained from the industrial production. The molecules crystallize as centrosymmetic dimers connected by two symmetry-related N-H center dot center dot center dot O = C hydrogen bonds. Each molecule also contains an intramolecular N-H center dot center dot center dot O = C hydrogen bond. The dimers form stacks along the a-axis direction. Neighbouring stacks are arranged into a herringbone structure.
引用
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页码:O2468 / +
页数:11
相关论文
共 17 条
[1]  
*BRUK AXS INC, 2000, SADABS
[2]   ANTITUMOR IMIDAZOTETRAZINES .32. SYNTHESIS OF NOVEL IMIDAZOTETRAZINONES AND RELATED BICYCLIC HETEROCYCLES TO PROBE THE MODE OF ACTION OF THE ANTITUMOR DRUG TEMOZOLOMIDE [J].
CLARK, AS ;
DEANS, B ;
STEVENS, MFG ;
TISDALE, MJ ;
WHEELHOUSE, RT ;
DENNY, BJ ;
HARTLEY, JA .
JOURNAL OF MEDICINAL CHEMISTRY, 1995, 38 (09) :1493-1504
[3]   METAL-ION COMPLEXATION BY A NEW UREA MACROCYCLOPHANE [J].
CORDIER, D ;
COULET, PR .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1994, (04) :891-894
[4]  
HERBST W, 2004, IND ORGANIC PIGMENTS, P260
[5]   Parallel synthesis and spectroscopic analysis of a collection of heterocycles based on the diazabenz[e]aceanthrylene core structure [J].
Jones, Alan M. ;
Lebl, Tomas ;
Patterson, Stephen ;
van Mourik, Tanja ;
Fruechtl, Herbert A. ;
Philp, Douglas ;
Slawin, Alexandra M. Z. ;
Westwood, Nicholas J. .
TETRAHEDRON, 2009, 65 (02) :563-578
[6]  
JUNG R, 2001, Patent No. 1188800
[7]   Lipase-catalyzed synthesis of a pure macrocyclic polyester from dimethyl terephthalate and diethylene glycol [J].
Lavalette, A ;
Lalot, T ;
Brigodiot, M ;
Maréchal, E .
BIOMACROMOLECULES, 2002, 3 (02) :225-228
[8]   Mercury CSD 2.0 -: new features for the visualization and investigation of crystal structures [J].
Macrae, Clare F. ;
Bruno, Ian J. ;
Chisholm, James A. ;
Edgington, Paul R. ;
McCabe, Patrick ;
Pidcock, Elna ;
Rodriguez-Monge, Lucia ;
Taylor, Robin ;
van de Streek, Jacco ;
Wood, Peter A. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2008, 41 :466-470
[9]  
METZ HJ, 1999, Patent No. 591057
[10]   Second-generation peptidomimetic inhibitors of protein farnesyltransferase demonstrating improved cellular potency and significant in vivo efficacy [J].
O'Connor, SJ ;
Barr, KJ ;
Wang, L ;
Sorensen, BK ;
Tasker, AS ;
Sham, H ;
Ng, SC ;
Cohen, J ;
Devine, E ;
Cherian, S ;
Saeed, B ;
Zhang, HC ;
Lee, JY ;
Warner, R ;
Tahir, S ;
Kovar, P ;
Ewing, P ;
Alder, J ;
Mitten, M ;
Leal, J ;
Marsh, K ;
Bauch, J ;
Hoffman, DJ ;
Sebti, SM ;
Rosenberg, SH .
JOURNAL OF MEDICINAL CHEMISTRY, 1999, 42 (18) :3701-3710