Utilisation of [11C]-labelled boron carbonyl complexes in palladium carbonylation reaction

被引：49

作者：

Audrain, H

Martarello, L

Gee, A

Bender, D

机构：

[1] Aarhus Univ Hosp, PET Ctr, DK-8000 Aarhus C, Denmark

[2] GlaxoSmithKline, Addenbrookes Hosp, Addenbrookes Ctr Clin Invest, Cambridge CB2 2GG, England

来源：

CHEMICAL COMMUNICATIONS | 2004年 / 05期

关键词：

D O I：

10.1039/b314982j

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The use of the [C-11]BH3.CO complex as a source of carbon monoxide in the carbonylation of iodobenzene catalysed by palladium(0) is described, which allows the synthesis of an amide and a lactone in a straightforward manner.

引用

页码：558 / 559

页数：2

共 12 条

[1]

Al-Qahtani MH, 2000, J LABELLED COMPD RAD, V43, P825, DOI 10.1002/1099-1344(200007)43:8<825::AID-JLCR367>3.0.CO

[2]

2-A

[3] Synthesis and properties of boranocarbonate:: A convenient in situ CO source for the aqueous preparation of [99mTC(OH2)3(CO)3]+ [J].

Alberto, R ;

Ortner, K ;

Wheatley, N ;

Schibli, R ;

Schubiger, AP .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (13) :3135-3136

[4] A remote-controlled high pressure reactor for radiotracer synthesis with [11C]carbon monoxide [J].

Hostetler, ED ;

Burns, HD .

NUCLEAR MEDICINE AND BIOLOGY, 2002, 29 (08) :845-848

[5] Biologically active 11C-labeled amides using palladium-mediated reactions with aryl halides and [11C]carbon monoxide [J].

Kihlberg, T ;

Långström, B .

JOURNAL OF ORGANIC CHEMISTRY, 1999, 64 (25) :9201-9205

[6] [11C]carbon monoxide in selenium-mediated synthesis of 11C-carbamoyl compounds [J].

Kihlberg, T ;

Karimi, F ;

Långström, B .

JOURNAL OF ORGANIC CHEMISTRY, 2002, 67 (11) :3687-3692

[7]

LIDSTROM P, 1997, J CHEM SOC P1, V18, P2701

[8] PALLADIUM-CATALYZED CROSS-COUPLING REACTIONS OF ORGANOBORON COMPOUNDS [J].

MIYAURA, N ;

SUZUKI, A .

CHEMICAL REVIEWS, 1995, 95 (07) :2457-2483

[9] PALLADIUM-MEDIATED CARBONYLATION AND COUPLING REACTIONS OF IODOBENZENE AND ANILINE - MODEL REACTIONS FOR THE PREPARATION OF AROMATIC POLYAMIDES [J].

PERRY, RJ ;

WILSON, BD .

MACROMOLECULES, 1993, 26 (07) :1503-1508

[10] Aryl triflates and [11C]/(13C)carbon monoxide in the synthesis of 11C-/13C-amides [J].

Rahman, O ;

Kihlberg, T ;

Långström, B .

JOURNAL OF ORGANIC CHEMISTRY, 2003, 68 (09) :3558-3562

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