Simple Electrochemical Determination of Hydrazine in Water

被引：8

作者：

Lauko, Lukas ^{[1
]}

Hudec, Roman ^{[1
]}

Lenghartova, Katarina ^{[2
]}

Manova, Alena ^{[1
]}

Cacho, Frantisek ^{[1
]}

Beinrohr, Ernest ^{[1
,2
]}

机构：

[1] Slovak Univ Technol Bratislava, Fac Chem & Food Technol, Inst Analyt Chem, Bratislava 81237, Slovakia

[2] Univ SS Cyril & Methodius Trnava, Fac Nat Sci, Dept Chem, Trnava 91701, Slovakia

来源：

POLISH JOURNAL OF ENVIRONMENTAL STUDIES | 2015年 / 24卷 / 04期

关键词：

hydrazine determination; boiler water; constant current chronopotentiometry; porous electrode; vitreous carbon; FLOW-INJECTION ANALYSIS; ELECTROCATALYTIC OXIDATION; VOLTAMMETRIC DETERMINATION; ELECTRODES; PLATINUM; COPPER; ELECTROOXIDATION; NANOPARTICLES;

D O I：

10.15244/pjoes/40935

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

Hydrazine in water samples is determined by constant current chronopotentiometry in porous carbon electrodes. Hydrazine in alkaline solutions is oxidised to nitrogen in the pores of the electrode by constant current. Two types of electrodes made of reticulated vitreous carbon (RVC) were used, one fabricated from crushed RVC particles, the other with the original RVC material of 100 ppi porosity. The former is suitable for hydrazine concentrations above 0.7 mg.dm(-3) up to 50 mg.dm(-3), the latter for the 8-700 mu g.dm(-3) range. The method was used for water samples, including boiler water.

引用

页码：1659 / 1666

页数：8

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