Microwave assisted green synthesis of pectin based silver nanoparticles and their antibacterial and antifungal activities

被引:38
作者
Su, Dong-lin [1 ,2 ,3 ,5 ]
Li, Pei-jun [2 ,3 ,4 ]
Ning, Meng [4 ]
Li, Gao-yang [2 ,3 ,5 ]
Shan, Yang [1 ,2 ,5 ]
机构
[1] Cent S Univ, Longping Branch, Grad Sch, Changsha 410125, Hunan, Peoples R China
[2] Hunan Acad Agr Sci, Hunan Agr Prod Proc Inst, Changsha 410125, Hunan, Peoples R China
[3] Hunan Key Lab Fruits & Vegetables Storage Proc &, Changsha 410125, Hunan, Peoples R China
[4] Guilin Univ Technol, Coll Chem & Bioengn, Guangxi Key Lab Electrochem & Magnetochem Funct M, Guilin 541004, Peoples R China
[5] Int Joint Lab Fruits & Vegetables Proc & Qual Saf, Changsha 410125, Hunan, Peoples R China
关键词
Spectroscopy; Nanoparticles; Microwave; Pectin; Antibacterial; ORANGE PEEL; EXTRACTION; ULTRASOUND; SIZE;
D O I
10.1016/j.matlet.2019.02.059
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this work, monodispersed silver nanoparticles (Ag NPs) were prepared by the reaction of silver nitrate with alkali hydrolyzed pectin at microwave irradiation. Two types of Ag NPs were obtained under the following conditions: 400W of microwave power, 1 g/l NaOH, 2 g/l pectin, 10 mmol/l AgNO3, and irradiation time for 1 and 2 min, respectively. The zeta potential values of Ag NPs colloidal solutions were -39.6 and -38.7 mV, indicating that these nanoparticles were stable. Transmission electron microscopy (TEM) analysis revealed these spherical Ag NPs with an average size 2.90 and 11.94 nm, respectively. Ag NPs exhibited potent antibacterial and antifungal activities to against Escherichia coli, Staphylococcus aureus, and Aspergillus japonicus, and the minimum bactericidal concentrations (MIC) to against E. coli and S. aureus were equally at 80-160 mg/ml. In a word, this is a green, efficient, and cost-effective method for Ag NPs synthesis. (C) 2019 Elsevier B.V. All rights reserved.
引用
收藏
页码:35 / 38
页数:4
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