Preparation of continuous alumina gel fibres by aqueous sol-gel process

被引:22
作者
Tan, Hongbin [1 ]
Ma, Xiaoling [1 ]
Fu, Mingxing [1 ]
机构
[1] Shaanxi Univ Technol, Sch Mat Sci & Engn, Hanzhong 723003, Shaanxi, Peoples R China
关键词
Continuous gel fibre; sol-gel method; Al2O3; polyvinylpyrrolidone; PRECURSOR; MICROSTRUCTURE; GAMMA-AL2O3; BEHAVIOR; GLASSES; MULLITE; POWDERS; LACTATE;
D O I
10.1007/s12034-013-0428-5
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Continuous alumina gel fibres were prepared by sol-gel method. The spinning sol was prepared by mixing aluminum nitrate, lactic acid and polyvinylpyrrolidone with a mass ratio of 10:3:1 center dot 5. Thermogravimetry-differential scanning calorimetry (TG-DSC), Fourier transform infrared (FTIR) spectra, X-ray diffraction (XRD), and scanning electron microscopy (SEM) were used to characterize the properties of the gel and ceramic fibres. The Al2O3 fibres with a uniform diameter can be obtained by sintering gel fibres at 1200 A degrees C.
引用
收藏
页码:153 / 156
页数:4
相关论文
共 19 条
[1]   Solubilities and vapour pressures of water over saturated solutions of magnesium-L-lactate, calcium-L-lactate, zinc-L-lactate, ferrous-L-lactate and aluminum-L-lactate [J].
Apelblat, A ;
Manzurola, E ;
van Krieken, J ;
Nanninga, GL .
FLUID PHASE EQUILIBRIA, 2005, 236 (1-2) :162-168
[2]   Sol-gel processing of alumina fibres [J].
Chandradass, J ;
Balasubramanian, M .
JOURNAL OF MATERIALS PROCESSING TECHNOLOGY, 2006, 173 (03) :275-280
[3]  
Karst K. A., 1977, U.S. Patent, Patent No. [4,047,965, 4047965]
[4]   Influence of thermal treatment conditions on the formation of phase-pure mullite derived from a nanoparticulate aluminosilicate precursor [J].
Leivo, Jarkko ;
Linden, Mika ;
Ritola, Merja ;
Vippola, Minnamari ;
Levanen, Erkki ;
Mantyla, Tapio A. .
MATERIALS CHEMISTRY AND PHYSICS, 2009, 115 (01) :56-64
[5]   Synthesis and sintering behavior of a nanocrystalline α-alumina powder [J].
Li, JG ;
Sun, XD .
ACTA MATERIALIA, 2000, 48 (12) :3103-3112
[6]   Low temperature synthesis of ultrafine α-Al2O3 powder by a simple aqueous sol-gel process [J].
Li, Jiang ;
Pan, Yubai ;
Xiang, Changshu ;
Ge, Qiming ;
Guo, Jingkun .
CERAMICS INTERNATIONAL, 2006, 32 (05) :587-591
[7]   Continuous hollow alumina gel fibers by direct electrospinning of an alkoxide-based precursor [J].
Maneeratana, Vasana ;
Sigmund, Wolfgang M. .
CHEMICAL ENGINEERING JOURNAL, 2008, 137 (01) :137-143
[8]   Sintering of α-Al2O3-seeded nanocrystalline γ-Al2O3 powders [J].
Nordahl, CS ;
Messing, GL .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2002, 22 (04) :415-422
[9]   Thermal analysis of phase transformation kinetics in α-Al2O3 seeded boehmite and γ-Al2O3 [J].
Nordahl, CS ;
Messing, GL .
THERMOCHIMICA ACTA, 1998, 318 (1-2) :187-199
[10]   Characterisation of stoichiometric sol-gel mullite by fourier transform infrared spectroscopy [J].
Padmaja, P ;
Anilkumar, GM ;
Mukundan, P ;
Aruldhas, G ;
Warrier, KGK .
INTERNATIONAL JOURNAL OF INORGANIC MATERIALS, 2001, 3 (07) :693-698