Attapulgite-Fe3O4 magnetic nanoparticles via co-precipitation technique

被引:160
作者
Liu, Yushan [1 ,2 ]
Liu, Peng [1 ,2 ]
Su, Zhixing [1 ,2 ]
Li, Fashen [3 ]
Wen, Fusheng [3 ]
机构
[1] Lanzhou Univ, Coll Chem & Chem Engn, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China
[2] Lanzhou Univ, Coll Chem & Chem Engn, Inst Polymer Sci & Engn, Lanzhou 730000, Peoples R China
[3] Lanzhou Univ, Minist Educ, Key Lab Magnetism & Magnet Mat, Lanzhou 730000, Peoples R China
关键词
Attapulgite; Fe3O4; Magnetic nanocomposite particles; Co-precipitation; Inorganic-inorganic nanoparticles;
D O I
10.1016/j.apsusc.2008.06.193
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The attapulgite/Fe3O4 magnetic nanoparticles (ATP-Fe3O4) were prepared by co-precipitation technique in the aqueous suspension of attapulgite pre-modified with FeCl3. The co-precipitation occurred by ammonia in presence of ferrous chloride at 90 degrees C under magnetic stirring. Morphology observation showed that the Fe3O4 nanoparticles were absorbed to attapulgite nano-needles' surfaces and their dispersibilities in water was also studied. The ATP-Fe3O4 particles had been characterized with Fourier transform infrared (FT-IR) spectroscopy analysis, X-ray diffraction (XRD), pore surface area (BET), transmission electron microscopy (TEM) and vibrating sample magnetometer (VSM). (C) 2008 Elsevier B. V. All rights reserved.
引用
收藏
页码:2020 / 2025
页数:6
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