Impacts of Egg White Assisted Combustion and Ceramic Methods on Structural, Morphological and Magnetic Properties of Nickel Manganite System
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作者:
Deraz, Nasrallah
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Natl Res Ctr, Phys Chem Dept, El Behooth St, Giza 12622, EgyptNatl Res Ctr, Phys Chem Dept, El Behooth St, Giza 12622, Egypt
Deraz, Nasrallah
[1
]
Abd-Elkader, Omar Hamed
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King Saud Univ, Sci Coll, Phys & Astron Dept, POB 2455, Riyadh 11451, Saudi Arabia
Natl Res Ctr, Electron Microscope & Thin Films Dept, Phys Div, El Behooth St, Giza 12622, EgyptNatl Res Ctr, Phys Chem Dept, El Behooth St, Giza 12622, Egypt
Abd-Elkader, Omar Hamed
[2
,3
]
Yassin, Mohamed
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King Saud Univ, Sci Coll, Bot & Microbiol Dept, POB 2455, Riyadh 11451, Saudi ArabiaNatl Res Ctr, Phys Chem Dept, El Behooth St, Giza 12622, Egypt
Yassin, Mohamed
[4
]
机构:
[1] Natl Res Ctr, Phys Chem Dept, El Behooth St, Giza 12622, Egypt
[2] King Saud Univ, Sci Coll, Phys & Astron Dept, POB 2455, Riyadh 11451, Saudi Arabia
[3] Natl Res Ctr, Electron Microscope & Thin Films Dept, Phys Div, El Behooth St, Giza 12622, Egypt
[4] King Saud Univ, Sci Coll, Bot & Microbiol Dept, POB 2455, Riyadh 11451, Saudi Arabia
This study focuses on two different techniques for preparation of nickel manganite (NiMn2O4) system. One approach is conventional ceramic method, and the second is based on replacing the ceramic route with green synthesis mediated by egg white. The goal of this strategy is produce a single nanomagnetic phase of NiMn(2)O(4)using a mostly simple one-step method with specific characteristics as seen in the second route compared to the ceramic method. The as synthesized system was characterized by using various techniques such as X-ray diffraction (XRD), scanning electron micrographs (SEM), and Energy dispersive X-ray spectrometry (EDS). XRD, EDS and SEM analyses confirm a successful synthesis of NiMn(2)O(4)single phase with cubic spinel and sponge crystal structures. The particles are polycrystalline in their nature and average crystallite size ranged between 76 and 90 nm. Egg white assisted combustion method imparted amelioration in the system crystallization, size of grain, distribution of cation and magnetic properties of the as prepared materials. The magnetic mensuration suggested that the obtained nickel manganite shows ferromagnetism at room temperature with an optimum value (3.56 emu/g) of saturation magnetization.
机构:
Bharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, IndiaBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
Shanmugavani, A.
Selvan, R. Kalai
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Bharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, IndiaBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
Selvan, R. Kalai
Layek, Samar
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Indian Inst Technol, Dept Phys, Kanpur 208016, Uttar Pradesh, IndiaBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
Layek, Samar
Vasylechko, Leonid
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Lviv Polytech Natl Univ, Semicond Elect Dept, UA-79013 Lvov, UkraineBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
Vasylechko, Leonid
Sanjeeviraja, C.
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Alagappa Chettiar Coll Engn & Technol, Dept Phys, Karaikkudi 630004, Tamil Nadu, IndiaBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
机构:
Bharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, IndiaBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
Shanmugavani, A.
Selvan, R. Kalai
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Bharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, IndiaBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
Selvan, R. Kalai
Layek, Samar
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Indian Inst Technol, Dept Phys, Kanpur 208016, Uttar Pradesh, IndiaBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
Layek, Samar
Vasylechko, Leonid
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Lviv Polytech Natl Univ, Semicond Elect Dept, UA-79013 Lvov, UkraineBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India
Vasylechko, Leonid
Sanjeeviraja, C.
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Alagappa Chettiar Coll Engn & Technol, Dept Phys, Karaikkudi 630004, Tamil Nadu, IndiaBharathiar Univ, Dept Phys, Solid State Ion & Energy Devices Lab, Coimbatore 641046, Tamil Nadu, India