Effect of Sintering Temperature on the Microstrutcure and Magnetic Properties of Fe-6.5%Si Alloy Fabricated by Metal Injection Molding

被引:7
作者
Choi, Dae Yeob [1 ]
Syarif, Husein [1 ]
Shin, Dong Hyuk [2 ]
Ko, Young Gun [1 ]
机构
[1] Yeungnam Univ, Sch Mat Sci & Engn, Kyongsan 712749, South Korea
[2] Hanyang Univ, Dept Met & Mat Engn, Ansan 426791, South Korea
来源
KOREAN JOURNAL OF METALS AND MATERIALS | 2013年 / 51卷 / 02期
关键词
metals; sintering; metal injection molding; magnetic properties; scanning electron microscopy; GRAIN-SIZE; DIFFUSION; BEHAVIOR; STEEL; MICROSTRUCTURE; MECHANISMS;
D O I
10.3365/KJMM.2013.51.2.105
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The present work demonstrated the influence of sintering temperature on the microstructure and magnetic properties of Fe-6.5%Si alloys fabricated via metal injection molding. The samples were sintered in an Ar atmosphere at three different temperatures, 1100, 1200, and 1300 degrees C. Microstructural observations of the sintered sample revealed that, with increasing sintering temperature, the average grain size of the ferrite phase increased, while the fraction of the micro pore decreased. These results were attributed to the increasing mobility of the grain boundaries. The hysteresis curves showed that the magnetic properties of the sintered samples as a soft magnet were enhanced with increasing sintering temperature since the saturation magnetization increased and the coercivity decreased, reaching the values of 1.22 tesla and 1.84 kA/m at 1300 degrees C. Moreover, the values of the magnetic hysteresis loss in the sintered samples gradually decreased with increasing sintering temperature due to both the fairly high densification and coarse grain size of the sintered sample.
引用
收藏
页码:105 / 111
页数:7
相关论文
共 26 条
[21]   PORE-BOUNDARY INTERACTIONS AND EVOLUTION-EQUATIONS FOR THE POROSITY AND THE GRAIN-SIZE DURING SINTERING [J].
SVOBODA, J ;
RIEDEL, H .
ACTA METALLURGICA ET MATERIALIA, 1992, 40 (11) :2829-2840
[22]   COMMERCIAL SCALE PRODUCTION OF FE-6.5 WT-PERCENT SI SHEET AND ITS MAGNETIC-PROPERTIES [J].
TAKADA, Y ;
ABE, M ;
MASUDA, S ;
INAGAKI, J .
JOURNAL OF APPLIED PHYSICS, 1988, 64 (10) :5367-5369
[23]   Effects of crystal grain size and particle size on core loss for Fe-Si compressed cores [J].
Takemoto, Satoshi ;
Saito, Takanobu .
PROGRESS IN POWDER METALLURGY, PTS 1 AND 2, 2007, 534-536 :1313-+
[24]   Die Compaction and Sintering Behavior of Fe Micro-nano-powder Feedstock for Micro-PIM [J].
You, Woo-Kyung ;
Choi, Joon-Phil ;
Lee, Jai-Sung .
KOREAN JOURNAL OF METALS AND MATERIALS, 2011, 49 (01) :32-39
[25]   Characterization of the evaluation of the solid solubility of Si in sintered Fe-Si alloys using DSC technique [J].
Yuan, W. J. ;
Li, R. ;
Shen, Q. ;
Zhang, L. M. .
MATERIALS CHARACTERIZATION, 2007, 58 (04) :376-379
[26]  
[No title captured]