Ultrasound-Assisted and One-Pot Synthesis of New Fe3O4/Mo-MOF Magnetic Nano Polymer as a Strong Antimicrobial Agent and Efficient Nanocatalyst in the Multicomponent Synthesis of Novel Pyrano[2,3-d]pyrimidines Derivatives

被引：21

作者：

Abdtawfeeq, Tarik Hafdhi ^{[1
]}

Farhan, Zainab A. ^{[2
]}

Al-Majdi, Kadhum ^{[3
]}

Jawad, Mohammed Abed ^{[4
]}

Zabibah, Rahman S. ^{[5
]}

Riadi, Yassine ^{[6
]}

Hadrawi, Salema K. ^{[7
]}

AL-Alwany, Ameen ^{[8
]}

Shams, Marwah A. ^{[9
]}

机构：

[1] Al Farahidi Univ, Med Tech Coll, Baghdad, Iraq

[2] Al Mustaqbal Univ Coll, Air conditioning & Refrigerat Tech Engn Dept, Babylon, Iraq

[3] Ashur Univ Coll, Dept Biomed Engn, Baghdad, Iraq

[4] Al Nisour Univ Coll, Baghdad, Iraq

[5] Islamic Univ, Coll Med Technol, Med Lab Technol Dept, Najaf, Iraq

[6] Prince Sattam Bin Abdulaziz Univ, Coll Pharm, Dept Pharmaceut Chem, Al Kharj 11942, Saudi Arabia

[7] Islamic Univ, Coll Tech Engn, Refrigerat & Air Conditioning Tech Engn Dept, Najaf, Iraq

[8] Univ Baghdad, Coll Med, Baghdad, Iraq

[9] Al Ayen Univ, Tech Engn Coll, Thi Qar, Iraq

来源：

JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS | 2023年 / 33卷 / 02期

关键词：

Ultrasound-assisted; Metal-organic framework; Fe3O4; Mo-MOF; Core shell nanoparticles; Magnetic nanocatalyst; Pyrano[2; 3-d]pyrimidines; Antimicrobial properties; CATALYST; NANOPARTICLES; GREEN; COORDINATION; HETEROCYCLES; PERFORMANCE; DESIGN;

D O I：

10.1007/s10904-022-02514-7

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

A new Fe3O4/Mo-MOF (metal-organic framework) magnetic nano polymer was synthesized in one step and Ultrasound assisted. Fe3O4/Mo-MOF magnetic nano polymer was characterized by XRD, SEM, EDX mapping BET, VSM, and FT-IR. The results of the structure confirmation revealed that the ultrasonic method had created unique properties in the Fe3O4/Mo-MOF magnetic nano polymer, and its biological and catalytic applications were investigated. A new pyrano[2,3-d]pyrimidines derivative was synthesized using the catalytic activity of Fe3O4/Mo-MOF magnetic nano polymer in a three-component reaction involving malononitrile, aldehyde derivatives, and barbituric acid derivatives with Fe3O4/Mo-MOF magnetic nano polymer as a magnetic catalyst. In the antimicrobial activity of Fe3O4/Mo-MOF magnetic nano polymer: Antimicrobial properties on gram-positive, gram-negative, and fungal strains based on MIC, MBC, and MFC value. The results of catalytic and biological studies proved that nanoparticles have unique properties attributed to their structure and synthesis method.

引用

页码：472 / 483

页数：12

共 70 条

[41] Green cellulose-based nanocomposite catalyst: Design and facile performance in aqueous synthesis of pyranopyrimidines and pyrazolopyranopyrimidines [J].