Single particle inductively coupled plasma mass spectrometry and its variations for the analysis of nanoparticles

被引:1
作者
Zhou, Zichao [1 ]
Beauchemin, Diane [1 ]
机构
[1] Queens Univ, Dept Chem, 90 Bader Lane, Kingston, ON K7L 3N6, Canada
基金
加拿大自然科学与工程研究理事会;
关键词
SAMPLE INTRODUCTION SYSTEM; MIXED-GAS PLASMA; SILVER NANOPARTICLES; ICP-MS; COLLOID ANALYSIS; FLOW-INJECTION; PLATINUM NANOPARTICLES; TRANSPORT EFFICIENCY; NUMBER CONCENTRATION; SIZE;
D O I
10.1039/d3cc04974d
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Single particle inductively coupled plasma mass spectrometry (spICPMS) can count and weigh metal-containing nanoparticles (NPs), enabling their sizing if their geometry, density, and composition are known. With a nebulizer and a spray chamber for sample introduction, both the sample uptake rate and the transport efficiency must be determined when calibrating with solutions. In contrast, flow injection (FI) and mono-segmented flow analysis (MSFA) coupled to spICPMS do not need determination of the transport efficiency and sample uptake rate for accurate NP mass measurement. Correcting for the significant settling time on some instruments is also discussed, as well as calibration through signal integration instead of averaging, which eliminates the need to measure the transport efficiency when seeking NP mass. Nitrogen added to the outer plasma gas can reduce the background for the determination of P, S, Ca and Fe. Infrared heating of the sample introduction system provides 100% transport efficiency, enabling accurate particle mass and concentration measurements without measurement of transport efficiency. Single particle inductively coupled plasma mass spectrometry (spICPMS) can count and weigh metal-containing nanoparticles (NPs), enabling their sizing if their geometry, density, and composition are known.
引用
收藏
页码:1826 / 1839
页数:15
相关论文
共 50 条
[41]   Determination of Silver Nanoparticles in Toothpaste by Single Particle-Inductively Coupled Plasma-Mass Spectrometry with Ultrasonic Extraction [J].
Shi, Rui-Xin ;
Zhao, Yon-Ping ;
Guan, Peng ;
Liang, Wei-Xin ;
Xun, He .
CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2020, 48 (04) :523-529
[42]   Determining Transport Efficiency for the Purpose of Counting and Sizing Nanoparticles via Single Particle Inductively Coupled Plasma Mass Spectrometry [J].
Pace, Heather E. ;
Rogers, Nicola J. ;
Jarolimek, Chad ;
Coleman, Victoria A. ;
Higgins, Christopher P. ;
Ranville, James F. .
ANALYTICAL CHEMISTRY, 2011, 83 (24) :9361-9369
[43]   Effect of Data Acquisition Parameters on Characterization of Gold Nanoparticles By Single Particle Inductively Coupled Plasma-Mass Spectrometry [J].
Luo Rui-Ping ;
Zheng Ling-Na ;
Li Liang ;
Wang Juan ;
Feng Wei-Yue ;
Yu Xiang-Hua ;
Wang Meng .
CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2018, 46 (06) :925-930
[44]   Electrospray-Differential Mobility Hyphenated with Single Particle Inductively Coupled Plasma Mass Spectrometry for Characterization of Nanoparticles and Their Aggregates [J].
Tan, Jiaojie ;
Liu, Jingyu ;
Li, Mingdong ;
El Hadri, Hind ;
Hackley, Vincent A. ;
Zechariah, Michael R. .
ANALYTICAL CHEMISTRY, 2016, 88 (17) :8548-8555
[45]   Validation of a Method for Surveillance of Nanoparticles in Mussels Using Single-Particle Inductively Coupled Plasma-Mass Spectrometry [J].
Bruvold, Are ;
Valdersnes, Stig ;
Loeschner, Katrin ;
Bienfait, Andre Marcel .
JOURNAL OF AOAC INTERNATIONAL, 2024, 107 (04) :608-616
[46]   Optimisation and application of an analytical approach for the characterisation of TiO2 nanoparticles in food additives and pharmaceuticals by single particle inductively coupled plasma-mass spectrometry [J].
Givelet, Lucas ;
Truffier-Boutry, Delphine ;
Noel, Laurent ;
Damlencourt, Jean-Francois ;
Jitaru, Petru ;
Guerin, Thierry .
TALANTA, 2021, 224
[47]   Gold colloid analysis by inductively coupled plasma-mass spectrometry in a single particle mode [J].
Degueldre, C ;
Favarger, PY ;
Wold, S .
ANALYTICA CHIMICA ACTA, 2006, 555 (02) :263-268
[48]   Main Strategies of the Sample Preparation of Biological Samples Containing Nanoparticles for Their Subsequent Analysis by Single Particle Inductively Coupled Plasma Mass Spectrometry: A Mini-Review [J].
Grebneva-Balyuk, O. N. ;
Kiseleva, M. S. ;
Kubrakova, I. V. .
JOURNAL OF ANALYTICAL CHEMISTRY, 2025, 80 (04) :608-622
[49]   Exploring the boundaries in the analysis of large particles by single particle inductively coupled plasma mass spectrometry: application to nanoclays [J].
Ojeda, David ;
Bolea, Eduardo ;
Perez-Arantegui, Josefina ;
Laborda, Francisco .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 2022, 37 (07) :1501-1511
[50]   Quantitative Analysis of Gold Nanoparticles in Single Cells by Laser Ablation Inductively Coupled Plasma-Mass Spectrometry [J].
Wang, Meng ;
Zheng, Ling-Na ;
Wang, Bing ;
Chen, Han-Qing ;
Zhao, Yu-Liang ;
Chai, Zhi-Fang ;
Reid, Helen J. ;
Sharp, Barry L. ;
Feng, Wei-Yue .
ANALYTICAL CHEMISTRY, 2014, 86 (20) :10252-10256