Characterizing the Thermally Grown Oxide in Thermal Barrier Coating by Terahertz Time Domain Spectroscopy

被引:6
|
作者
Zhao, Wenhan [1 ]
Wang, Shibin [2 ]
Li, Lin'an [2 ]
Liu, Delin [2 ]
Li, Chuanwei [2 ]
Wang, Zhiyong [2 ]
机构
[1] Tianjin Univ, Dept Mech, Tianjin 300072, Peoples R China
[2] Beijing Inst Aeronaut Mat, Aviat Key Lab Sci & Technol Adv Corros & Protect A, Beijing 100094, Peoples R China
基金
中国国家自然科学基金;
关键词
non-destructive; thermal barrier coatings; terahertz time-domain spectroscopy; thermally grown oxide; optimization algorithm; SEM observation; IN INFRARED THERMOGRAPHY; THICKNESS;
D O I
10.3390/coatings13020376
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
This paper presents a method to simultaneously measure the thickness and refractive index of the thermally grown oxide (TGO) in thermal barrier coating (TBC) by using a reflective terahertz time-domain spectroscopy (THz-TDS) system. First, an optical transmission model of THz radiation in the multilayer structure of TBC is established. Owing to the different structures of TBC before and after forming the TGO layer, two different transmission models are established, respectively. Then, the experimental signals from the samples after different thermal cycles are obtained by the THz-TDS system. By fitting the experimentally measured reflected THz signals from the TBC samples to the proposed optical model using an optimization algorithm, the thickness and refractive index of the TGO are determined. In this work, four samples with different thicknesses of TGO layers are analyzed. The results of thickness of TGO layer are verified by SEM observation, and a reasonable agreement is obtained.
引用
收藏
页数:9
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