Microstructures and tribological properties of MoS2 overlayers on MAO Al alloy

被引:22
作者
Li, Weizhou [1 ,3 ]
Yan, Zhibin [2 ,3 ]
Shen, Deli [1 ]
Zhang, Ziying [3 ]
Yang, Ruixia [2 ,3 ]
机构
[1] Xiamen Univ Technol, Sch Mat Sci & Engn, Xiamen 361024, Peoples R China
[2] South China Univ Technol, Sch Mat Sci & Engn, Guangzhou 510640, Peoples R China
[3] Guangxi Univ, Sch Resources Environm & Mat, Nanning 530004, Peoples R China
关键词
MoS2; Tribological properties; Self-lubricating; Micro-arc oxidation (MAO); NANOSHEETS; PERFORMANCE; SPHERES;
D O I
10.1016/j.triboint.2023.108348
中图分类号
TH [机械、仪表工业];
学科分类号
0802 ;
摘要
To improve tribological properties of micro-arc oxidation (MAO) coating, MoS2 overlayers with self-lubricating effect were prepared by hydrothermal synthesis. The results showed that MoS2/MAO coating was mainly composed of MoS2, gamma-Al2O3 and mullite phases. With an increase of hydrothermal temperature, crystallinity, thickness and continuity of the MoS2 overlayer were increased. E2 g/A1 g ratio in the Raman spectra experienced a decrease from 0.738 to 0.493. XPS and TEM analysis discovered that oxygen was incorporated into the MoS2 at lower hydrothermal temperature from incomplete decomposition of MoO42-. Wear tests evidenced a lower average COF and better self-lubricating effect in the MoS2 synthesized at lower temperature. It was concluded that oxygen-incorporation into the MoS2 improved self-lubricating effect due to alignment to basal-plane orientation.
引用
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页数:19
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