Effect of TiB2 content on microstructure and mechanical properties of SiC composite ceramics by solid-state spark plasma sintering

被引:2
作者
Liu, Jiangao [1 ,2 ]
Li, Yang [1 ,2 ]
Cheng, Changgui [1 ,2 ]
Li, Wei [1 ,2 ]
机构
[1] Wuhan Univ Sci & Technol, State Key Lab Refractories & Met, Wuhan 430081, Peoples R China
[2] Wuhan Univ Sci & Technol, Key Lab Ferrous Met & Resources Utilizat, Minist Educ, Wuhan 430081, Peoples R China
基金
中国国家自然科学基金;
关键词
SiC-TiB2; Spark plasma sintering; Microstructure; Mechanical property; SIC-TIB2; COMPOSITES; MATRIX COMPOSITES; SILICON; MICROCRACKING; TOUGHNESS; BEHAVIOR; CARBON;
D O I
10.1007/s41779-023-00966-9
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
SiC-TiB2 composite ceramics of the solid-state has stable property in high temperature with wide application. In the paper, SiC-TiB2 composite ceramics was prepared by spark plasma sintering with 50 MPa pressure and heat preservation for 10 min at 1750 C-degrees, and the effect of TiB2 content (0 vo l%-20 vol%) on microstructure and mechanical properties of SiC composite ceramics by solid-state spark plasma sintering was investigated. The experimental results show that the grain growth of SiC is inhibited with the increase of TiB2 content. When TiB2 content is 20 vol%, TiB2 promotes the decomposition of SiC into Si, which is located in the grain boundaries of SiC and TiB2 to reduce mechanical properties of composite ceramics. SiC-15 vo l%TiB2 composite ceramics have the preferable comprehensive mechanical properties with relative density, Vickers hardness, bending strength and fracture toughness of 98.8%, 27.2 GPa, 431 MPa and 5.24 MPa center dot m(1/2), respectively.
引用
收藏
页码:971 / 978
页数:8
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