The 3-(2-Chloroethoxy)-1-(4-methoxyphenyl)-1H-pyrazole-4-carbaldehyde

被引：1
|
作者：
Varvuolyte, Gabriele [1 ,2 ]
Bieliauskas, Aurimas [2 ]
Kleiziene, Neringa [2 ]
Zukauskaite, Asta [1 ,3 ]
Sackus, Algirdas [1 ,2 ]
机构：
[1] Kaunas Univ Technol, Dept Organ Chem, LT-50254 Kaunas, Lithuania
[2] Kaunas Univ Technol, Inst Synthet Chem, LT-51423 Kaunas, Lithuania
[3] Palacky Univ, Fac Sci, Dept Chem Biol, CZ-78371 Olomouc, Czech Republic
来源：
MOLBANK | 2024年 / 2024卷 / 01期
关键词：
Vilsmeier-Haack reaction; pyrazole; aldehyde; dual functionalization; VILSMEIER-HAACK; DYES;
D O I：
10.3390/M1782
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Herein, we describe the synthesis of 3-(2-chloroethoxy)-1-(4-methoxyphenyl)-1H-pyrazole-4-carbaldehyde via the Vilsmeier-Haack reaction. The structure of this previously unreported compound is thoroughly elucidated through NMR, FT-IR spectroscopy and HRMS spectrometry.
引用
收藏
页数：5
相关论文
共 50 条
  • [21] 1-(4-Chlorophenyl)-3-(4-methoxyphenyl)prop-2-en-1-one
    Harrison, WTA
    Yathirajan, HS
    Sarojini, BK
    Narayana, B
    Indira, J
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O1647 - O1649
  • [22] 1-(4-Bromophenyl)-3-(4-methoxyphenyl)prop-2-en-1-one
    Shettigar, Venkataraya
    Rosli, Mohd Mustaqim
    Fun, Hoong-Kun
    Razak, Ibrahim Abdul
    Patil, P. S.
    Dharmaprakash, S. M.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4128 - O4129
  • [23] 1-(4-hydroxyphenyl)-3-(4-methoxyphenyl)prop-2-en-1-one
    Moorthi, SS
    Chinnakali, K
    Nanjundan, S
    Radhika, R
    Fun, HK
    Yu, XL
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O480 - O482
  • [24] 1-(4-fluorophenyl)-3-(4-methoxyphenyl)prop-2-en-1-one
    Harrison, William T. A.
    Yathirajan, H. S.
    Anilkumar, H. G.
    Sarojini, B. K.
    Narayana, B.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O3251 - O3253
  • [25] Crystal structure of ethyl 3-(4-methoxyphenyl)-1-(2-(4-methoxyphenyl)-2-oxoethyl)-1H-pyrazole-5-carboxylate, C22H22N2O5
    Zhou, Jinhui
    Zheng, Liangwen
    Liu, Jing
    Guo, Yongen
    Ding, Lin
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2017, 232 (04): : 679 - 680
  • [26] 1-{(E)-[3-(1H-Imidazol-1-yl)-1-(4-methoxyphenyl) propylidene] amino}-3-(2-methylphenyl) urea
    Attia, Mohamed I.
    Aboul-Enein, Mohamed N.
    El-Brollosy, Nasser R.
    Ng, Seik Weng
    Tiekin, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1799 - +
  • [27] 3-(4-Methoxyphenyl)-1H-isochromen-1-one
    Maiyalagan, T.
    Hathwar, Venkatesha R.
    Manivel, P.
    Arslan, N. Burcu
    Khan, F. Nawaz
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O128 - U2367
  • [28] 3-(4-Aminophenyl)-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazole-1-carbothioamide
    Suwunwong, Thitipone
    Chantrapromma, Suchada
    Kumar, C. S. Chidan
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1227 - +
  • [29] 5-(4-methoxybenzoyl)-4-(4-methoxyphenyl)-1-[1-(4-methoxyphenyl)ethylidenenamino]pyrimidin-2(1H)-one
    Özçelik, S
    Dinçer, M
    Saripinar, E
    Yilmaz, C
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O637 - O638
  • [30] 1-(4-Methoxyphenyl)-2-methyl-1H-indole-3-carbonitrile
    Yan, Qiao
    Qi, Xiuxiang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2312 - U2426
12345