Crystal structure of N-2,6-difluorobenzoyl-N′-[1-(3-chloro-4-methyl-phenyl)-4-cyano-1H-pyrazol-5-carbamoyl]urea, C19H12ClF2N5O2

被引:1
作者
Li, Nan [1 ]
Li, Zheng [1 ]
Wang, Tian Ci [3 ]
Miao, Jun [4 ]
Wu, Haixia [1 ]
Gao, Jin Long [1 ]
Shan, Ju Chuan [2 ]
机构
[1] Hebei Univ Sci & Technol, Coll Chem & Pharmaceut Engn, 26 Yuxiang St, Shijiazhuang 050018, Peoples R China
[2] Hebei Univ Sci & Technol, Coll Text & Garments, 26 Yuxiang St, Shijiazhuang 050018, Peoples R China
[3] PetroChina, Huanqing Oil Prod Co, Yumen Oilfield Co, Beijing, Peoples R China
[4] PetroChina, No 2 Oil Prod Co, Changqing Oilfield Co, Beijing, Peoples R China
来源
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2023年 / 238卷 / 02期
关键词
CHITIN SYNTHESIS;
D O I
10.1515/ncrs-2022-0569
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C19H12ClF2N5O2, monoclinic, P2(1)/n (no. 14), a = 14.405(9) angstrom, b = 7.579(5) angstrom, c = 17.610(9) angstrom, beta = 95.856(13)degrees, V = 1913(2) angstrom(3), Z = 4, R-gt(F) = 0.0464, wR(ref)(F-2) = 0.1134, T = 296 K.
引用
收藏
页码:193 / 195
页数:3
相关论文
共 13 条
[1]  
Bai Yunlong, 2021, Journal of Chinese Society for Corrosion and Protection, V41, P60, DOI 10.11902/1005.4537.2020.015
[2]  
Brandenburg K., 2015, VISUAL CRYSTAL STRUC
[3]  
Bruker, 2016, APEX3 and SAINT
[4]   Synthesis and bioassay evaluation of 1-(4-substitutedideneaminooxymethyl)-phenyl-3-(2,6-difluorobenzoyl)ureas [J].
Chen, Li ;
Ou, Xiao-Ming ;
Mao, Chun-Hui ;
Shang, Jian ;
Huang, Run-Qiu ;
Bi, Fu-Chun ;
Wang, Qing-Min .
BIOORGANIC & MEDICINAL CHEMISTRY, 2007, 15 (11) :3678-3683
[5]   OLEX2: a complete structure solution, refinement and analysis program [J].
Dolomanov, Oleg V. ;
Bourhis, Luc J. ;
Gildea, Richard J. ;
Howard, Judith A. K. ;
Puschmann, Horst .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2009, 42 :339-341
[6]   Effects of benzoylphenylurea on chitin synthesis and orientation in the cuticle of the Drosophila larva [J].
Gangishetti, Umesh ;
Breitenbach, Sophie ;
Zander, Mareike ;
Saheb, Shaik Khaleelulla ;
Mueller, Ursula ;
Schwarz, Heinz ;
Moussian, Bernard .
EUROPEAN JOURNAL OF CELL BIOLOGY, 2009, 88 (03) :167-180
[7]   STRUCTURE-ACTIVITY-RELATIONSHIPS OF BENZOYLPHENYL UREAS AS TOXICANTS AND CHITIN SYNTHESIS INHIBITORS IN ONCOPELTUS-FASCIATUS [J].
HAJJAR, NP ;
CASIDA, JE .
PESTICIDE BIOCHEMISTRY AND PHYSIOLOGY, 1979, 11 (1-3) :33-45
[8]   Crystal structure of flufenoxuron: a benzoylurea pesticide [J].
Jeon, Youngeun ;
Kang, Gihaeng ;
Lee, Sangjin ;
Kim, Tae Ho .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 :O1110-+
[9]  
Li Z, 1998, J CHEM RES-S, P478
[10]   Studies on the action mechanism of benzoylurea insecticides to inhibit the process of chitin synthesis in insects: A review on the status of research activities in the past, the present and the future prospects [J].
Matsumura, Fumio .
PESTICIDE BIOCHEMISTRY AND PHYSIOLOGY, 2010, 97 (02) :133-139