New biocompatible low modulus and high strength β Ti-Fe-Nb-Sn ultrafine eutectic composites

被引:3
作者
Rossi, Mariana C. [1 ]
Afonso, Conrado R. M. [1 ]
机构
[1] Univ Fed Sao Carlos UFSCar, Dept Engn Mat DEMa, Rodovia Washington Luis,km 235, BR-13565905 Sao Carlos, SP, Brazil
来源
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T | 2023年 / 27卷
基金
巴西圣保罗研究基金会;
关键词
beta Ti -Fe -Nb -Sn alloys; Ultrafine eutectic composites; Microstructural characterization; Mechanical properties; MECHANICAL-PROPERTIES; MICROSTRUCTURE; ALLOY; SYSTEM; CO;
D O I
10.1016/j.jmrt.2023.11.192
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
High strength beta Ti-Fe-Nb-Sn ultrafine eutectic composites are promising in structural and functional applica-tions exhibiting high fracture strength with large plasticity. The present work aims to develop new biocompatible beta Ti-Fe-based ultrafine eutectic composites using biocompatible elements (Ti, Fe, Sn and Nb) and avoiding and/ or controlling the formation of metastable omega phase also known as Laves phase. Five new compositions (Ti64Fe22Nb14, Ti66Nb18Fe16, Ti63Fe23Nb8Sn6, Ti(60)Fe(23)Nb(8)Sn(9 )and Ti44Fe34Nb16Sn6 (at.%) were produced using Cu-mold suction casting and the evolution of phases and microstructure with the cooling rate and their me-chanical properties were investigated. In this sense, was observed a decreasing in the melting point by the addition of eutectoid beta-stabilizing elements (Fe and Sn), which leads to values down to Tl = 1215 C-degrees. The samples were characterized by X-ray diffraction, differential scanning calorimetry, scanning and transmission electron microscopy, Young's modulus measurements by the ultrasonic method, microhardness and compression tests. Thus, in this paper are shown promising results on new biocompatible metallic alloys of the TiFeNbSn system with high strength and low Young's modulus due to the adequate combination of a microstructure formed by micrometer-sized beta-Ti dendrites with ultrafine eutectics between soft beta-Ti phase and hard Ti-Fe and Ti3Sn in-termetallics, highlighting alloys Ti64Fe22Nb14 and Ti63Fe23Nb8Sn6. Their yield and fracture strength measured by compression and Young's Modulus measured by ultrasound were 1810 MPa, 2160 MPa and 45 GPa for alloy Ti64Fe22Nb14 and 1915 MPa, 2240 MPa and 59 GPa for alloy Ti63Fe23Nb8Sn6 (at.%)
引用
收藏
页码:7695 / 7704
页数:10
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