A Sensitive Electrochemical Sensor for Tectoridin Detection Based on Reduced Graphene Oxide/Polyethyleneimine Modified Glassy Carbon Electrode

被引：2

作者：

Wei, Yingliang ^{[1
]}

Wang, Anting ^{[1
]}

Wang, Lu ^{[1
]}

Wang, Fang ^{[1
]}

机构：

[1] Luoyang Inst Sci & Technol, Sch Environm Engn & Chem, Luoyang 471023, Peoples R China

来源：

RUSSIAN JOURNAL OF ELECTROCHEMISTRY | 2023年 / 59卷 / 06期

基金：

中国国家自然科学基金;

关键词：

tectoridin; reduced graphene oxide; polyethyleneimine composite modified electrode; voltammetry; electrochemical behavior; BELAMCANDA-CHINENSIS L; POLY(ETHYLENIMINE); ACETAMINOPHEN; NANOPARTICLES; COMPOSITE; MERCURY; WATER; OXIDE;

D O I：

10.1134/S1023193523060071

中图分类号：

O646 [电化学、电解、磁化学];

学科分类号：

081704 ;

摘要：

Polyethyleneimine (PEI) functionalized reduced graphene oxide (rGO) was fabricated using PEI as the reducing agent of graphene oxide (GO), and characterized by Fourier transform infrared spectrum, electrochemical impedance spectroscopy. A sensitive electrochemical sensor was constructed based on rGO/PEI hybrid modified glassy carbon electrode (rGO/PEI/GCE) for the determination of tectoridin (TEC). The redox character of TEC at the proposed sensor was studied, and some electrochemical parameters were discussed. The electroanalytical method for the detection of TEC was established by cyclic voltammetry. Under optimized conditions, this proposed sensor showed a good linear relationship in the concentration range of 5.0 x 10(-7)-1.0 x 10(-5) mol/L. The recovery of TEC was 94.0-105.0%, which indicated that the accuracy of the proposed method was reliable. This sensor could be applied successfully to determine TEC in the Chinese medicinal herb Belamcanda chinensis and Flos Puerariae with satisfactory results.

引用

页码：473 / 480

页数：8

共 27 条

[1] APPLICATION OF POTENTIOSTATIC CURRENT INTEGRATION TO STUDY OF ADSORPTION OF COBALT(3)-)ETHYLENEDINITRILO)TETRAACETATE ON MERCURY ELECTRODES [J].

ANSON, FC .

ANALYTICAL CHEMISTRY, 1964, 36 (04) :932-&

[2] Ultrathin epitaxial graphite: 2D electron gas properties and a route toward graphene-based nanoelectronics [J].

Berger, C ;

Song, ZM ;

Li, TB ;

Li, XB ;

Ogbazghi, AY ;

Feng, R ;

Dai, ZT ;

Marchenkov, AN ;

Conrad, EH ;

First, PN ;

de Heer, WA .

JOURNAL OF PHYSICAL CHEMISTRY B, 2004, 108 (52) :19912-19916

[3] The use of polyethyleneimine-modified reduced graphene oxide as a substrate for silver nanoparticles to produce a material with lower cytotoxicity and long-term antibacterial activity [J].

Cai, Xiang ;

Lin, Minsong ;

Tan, Shaozao ;

Mai, Wenjie ;

Zhang, Yuanming ;

Liang, Zhiwen ;

Lin, Zhidan ;

Zhang, Xiuju .

CARBON, 2012, 50 (10) :3407-3415

[4] A new and simple method for the simultaneous determination of amoxicillin and nimesulide using carbon black within a dihexadecylphosphate film as electrochemical sensor [J].

Deroco, Patricia B. ;

Rocha-Filho, Romeu C. ;

Fatibello-Filho, Orlando .

TALANTA, 2018, 179 :115-123

[5] Four New Compounds Isolated from the Aerial Part of Belamcanda chinensis (L.) and Their Effect on Vascular Smooth Muscle Cell (VSMC) Proliferation [J].

Do Thi Ha ;

Bui Thi Binh ;

Nguyen Thi Thu ;

Nguyen Thi Bich Thu ;

Pham Ha Thanh Tung ;

Oh, Won Keun .

CHEMICAL & PHARMACEUTICAL BULLETIN, 2019, 67 (01) :41-46

[6] Interactions between Solid Surfaces with Preadsorbed Poly(ethylenimine) (PEI) Layers: Effect of Unadsorbed Free PEI Chains [J].

Gong, Xiangjun ;

Ngai, To .

LANGMUIR, 2013, 29 (20) :5974-5981

[7] Tectorigenin inhibits osteosarcoma cell migration through downregulation of matrix metalloproteinases in vitro [J].

Guo, Yu ;

Chen, Ya-Hong ;

Cheng, Zhi-Hua ;

Ou-Yang, Huo-Niu ;

Luo, Cong ;

Guo, Zhi-Lin .

ANTI-CANCER DRUGS, 2016, 27 (06) :540-546

[8] Isolation and purification of isoflavonoids from Rhizoma Belamcandae by two-dimensional preparative high-performance liquid chromatography with column switch technology [J].

Jiang, Yunyun ;

Zhao, Weiquan ;

Feng, Chao ;

Zhou, Tingting ;

Fan, Guorong ;

Wu, Yutian .

BIOMEDICAL CHROMATOGRAPHY, 2009, 23 (10) :1064-1072

[9] Study of substance changes in flowers of Pueraria thunbergiana Benth. during storage [J].

Kim, C ;

Shin, S ;

Ha, H ;

Kim, JM .

ARCHIVES OF PHARMACAL RESEARCH, 2003, 26 (03) :210-213

[10] Dispersion behaviour of graphene oxide and reduced graphene oxide [J].

Konios, Dimitrios ;

Stylianakis, Minas M. ;

Stratakis, Emmanuel ;

Kymakis, Emmanuel .

JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2014, 430 :108-112

← 1 2 3 →