Near ambient pressure-x-ray photoelectron spectroscopy spectra of lithium bis (trifluoromethane-sulfonyl) imide in propylene carbonate

被引:3
|
作者
Dietrich, Paul M. [1 ]
Gerlein, Lydia [2 ]
Maibach, Julia [2 ,3 ]
Thissen, Andreas [1 ]
机构
[1] SPECS Surface Nano Anal GmbH, Voltastr 5, D-13355 Berlin, Germany
[2] Karlsruhe Inst Technol KIT, Inst Appl Mat IAM ESS, Hermann von Helmholtz Pl 1, D-76344 Eggenstein Leopoldshafen, Germany
[3] Chalmers Univ Technol, Dept Phys, SE-41296 Gothenburg, Sweden
来源
SURFACE SCIENCE SPECTRA | 2023年 / 30卷 / 01期
关键词
Electrolyte; lithium salt; Li-ion battery; near ambient pressure x-ray photoelectron spectroscopy; NAP-XPS;
D O I
10.1116/6.0002435
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Near ambient pressure-x-ray photoelectron spectroscopy (NAP-XPS) is a less traditional form of XPS that allows samples to be analyzed at relatively high pressures, i.e., at greater than 5000 Pa. NAP-XPS can probe moderately volatile liquids, biological samples, porous materials, and/or polymeric materials that outgas significantly. In this submission, we show the survey, Li 1s, S 2p, C 1s, N 1s, O 1s, and F 1s NAP-XPS spectra of a Li-based electrolyte solution, which is a material that would be difficult to analyze by conventional XPS. The measurements were performed at 200 Pa in ambient gas atmosphere to compensate for surface charging. Peak fits of the C 1s, O 1s, and F 1s narrow scans are presented.
引用
收藏
页数:11
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