Near ambient pressure-x-ray photoelectron spectroscopy spectra of lithium bis (trifluoromethane-sulfonyl) imide in propylene carbonate

被引：3

作者：

Dietrich, Paul M. ^{[1
]}

Gerlein, Lydia ^{[2
]}

Maibach, Julia ^{[2
,3
]}

Thissen, Andreas ^{[1
]}

机构：

[1] SPECS Surface Nano Anal GmbH, Voltastr 5, D-13355 Berlin, Germany

[2] Karlsruhe Inst Technol KIT, Inst Appl Mat IAM ESS, Hermann von Helmholtz Pl 1, D-76344 Eggenstein Leopoldshafen, Germany

[3] Chalmers Univ Technol, Dept Phys, SE-41296 Gothenburg, Sweden

来源：

SURFACE SCIENCE SPECTRA | 2023年 / 30卷 / 01期

关键词：

Electrolyte; lithium salt; Li-ion battery; near ambient pressure x-ray photoelectron spectroscopy; NAP-XPS;

D O I：

10.1116/6.0002435

中图分类号：

O469 [凝聚态物理学];

学科分类号：

070205 ;

摘要：

Near ambient pressure-x-ray photoelectron spectroscopy (NAP-XPS) is a less traditional form of XPS that allows samples to be analyzed at relatively high pressures, i.e., at greater than 5000 Pa. NAP-XPS can probe moderately volatile liquids, biological samples, porous materials, and/or polymeric materials that outgas significantly. In this submission, we show the survey, Li 1s, S 2p, C 1s, N 1s, O 1s, and F 1s NAP-XPS spectra of a Li-based electrolyte solution, which is a material that would be difficult to analyze by conventional XPS. The measurements were performed at 200 Pa in ambient gas atmosphere to compensate for surface charging. Peak fits of the C 1s, O 1s, and F 1s narrow scans are presented.

引用

页数：11

共 19 条

[1] Oxygen gas, O2(g), by near-ambient pressure XPS [J].

Avval, Tahereh G. ;

Chatterjee, Shiladitya ;

Hodges, Grant T. ;

Bahr, Stephan ;

Dietrich, Paul ;

Meyer, Michael ;

Thissen, Andreas ;

Linford, Matthew R. .

SURFACE SCIENCE SPECTRA, 2019, 26 (01)

[2] Carbon dioxide gas, CO2(g), by near-ambient pressure XPS [J].

Avval, Tahereh G. ;

Chatterjee, Shiladitya ;

Bahr, Stephan ;

Dietrich, Paul ;

Meyer, Michael ;

Thissen, Andreas ;

Linford, Matthew R. .

SURFACE SCIENCE SPECTRA, 2019, 26 (01)

[3] Dimethyl sulfoxide by near-ambient pressure XPS [J].

Avval, Tahereh G. ;

Cushman, Cody V. ;

Bahr, Stephan ;

Dietrich, Paul ;

Meyer, Michael ;

Thissen, Andreas ;

Linford, Matthew R. .

SURFACE SCIENCE SPECTRA, 2019, 26 (01)

[4] Probing Lithium-Ion Battery Electrolytes with Laboratory Near-Ambient Pressure XPS [J].

Dietrich, Paul M. ;

Gehrlein, Lydia ;

Maibach, Julia ;

Thissen, Andreas .

CRYSTALS, 2020, 10 (11) :1-13

[5] Chemical surface analysis on materials and devices under functional conditions - Environmental photoelectron spectroscopy as non-destructive tool for routine characterization [J].

Dietrich, Paul M. ;

Bahr, Stephan ;

Yamamoto, Takashi ;

Meyer, Michael ;

Thissen, Andreas .

JOURNAL OF ELECTRON SPECTROSCOPY AND RELATED PHENOMENA, 2019, 231 :118-126

[6] Surface characterisation of Escherichia coli under various conditions by near-ambient pressure XPS [J].

Kjaervik, Marit ;

Schwibbert, Karin ;

Dietrich, Paul ;

Thissen, Andreas ;

Unger, Wolfgang E. S. .

SURFACE AND INTERFACE ANALYSIS, 2018, 50 (11) :996-1000

[7] Probing a battery electrolyte drop with ambient pressure photoelectron spectroscopy [J].

Maibach, Julia ;

Kallquist, Ida ;

Andersson, Margit ;

Urpelainen, Samuli ;

Edstrom, Kristina ;

Rensmo, Hakan ;

Siegbahn, Hans ;

Hahlin, Maria .

NATURE COMMUNICATIONS, 2019, 10 (1)

[8] Bacterial cellulose films with ZnO nanoparticles and propolis extracts: Synergistic antimicrobial effect [J].

Mocanu, Alexandra ;

Isopencu, Gabriela ;

Busuioc, Cristina ;

Popa, Oana-Maria ;

Dietrich, Paul ;

Socaciu-Siebert, Liana .

SCIENTIFIC REPORTS, 2019, 9 (1)

[9] Ethylene glycol, by near-ambient pressure XPS [J].

Patel, Dhananjay I. ;

O'Tani, James ;

Bahr, Stephan ;

Dietrich, Paul ;

Meyer, Michael ;

Thissen, Andreas ;

Linford, Matthew R. .

SURFACE SCIENCE SPECTRA, 2019, 26 (02)

[10] Ambient air, by near-ambient pressure XPS [J].

Patel, Dhananjay I. ;

Bahr, Stephan ;

Dietrich, Paul ;

Meyer, Michael ;

Thissen, Andreas ;

Linford, Matthew R. .

SURFACE SCIENCE SPECTRA, 2019, 26 (02)

← 1 2 →