3-Methyl-1-phenyl-4-thioacetylpyrazol-5-one

被引：0

作者：

Petkova, Zhanina ^{[1
]}

Rusew, Rusi ^{[2
]}

Shivachev, Boris ^{[2
]}

Kurteva, Vanya ^{[1
]}

机构：

[1] Bulgarian Acad Sci, Inst Organ Chem, Ctr Phytochem, Acad G Bonchev St,Bl 9, Sofia 1113, Bulgaria

[2] Bulgarian Acad Sci, Inst Mineral & Crystallog Acad Ivan Kostov, Acad G Bonchev St,Bl 107, Sofia 1113, Bulgaria

来源：

MOLBANK | 2023年 / 2023卷 / 01期

关键词：

3-methyl-1-phenyl-4-thioacetylpyrazol-5-one; acylpyrazolone; NMR; single-crystal XRD; COORDINATION CHEMISTRY; LAWESSONS REAGENT; METAL-COMPLEXES; EXTRACTION; SULFUR; LIGANDS;

D O I：

10.3390/M1588

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The novel compound 3-methyl-1-phenyl-4-thioacetylpyrazol-5-one is obtained in excellent yield via a thionation of the corresponding oxygen analogue. The product is isolated in pure form using column chromatography and is characterised using 1D and 2D NMR experiments, ATR IR and HRMS spectra, and single-crystal XRD.

引用

页数：7

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