Ferric and Ferrous Molar Ratio Effect on Physical and Magnetic Properties of Iron Oxide Nanoparticles

被引:0
作者
Mahaparale, Sonali P. [1 ]
Patil, Amruta R. [1 ]
机构
[1] Dr DY Patil Coll Pharm, Dept Pharmaceut Chem, Akurdi 411044, Pune, India
关键词
Ferric chloride; Ferrous sulphate; Iron oxide; Supermagnetic; Magnetic nanoparticles; FE3O4; NANOPARTICLES;
D O I
10.22068/ijmse.3532
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Iron oxide nanoparticles have been attracted extensively due to their supermagnetic properties, preferred in biomedicine because of their biocompatibility and potential nontoxicity to human beings. Synthesis of iron nanoparticles (FeNPs) was prepared with the help of ferric chloride and ferrous sulphate by using the coprecipitation method. The variation and combination of ferric and ferrous concentrations affect the physical and magnetic properties of iron oxide nanoparticles. The effect of 0.1 M ferric and ferrous concentration on iron oxide nanoparticles was studied separately and in combination. The obtained nanoparticles were characterized by Particle size, zeta potential, Ultraviolet (UV -visible), Fourier Transform Infrared Spectroscopy (FTIR), X-ray diffraction (XRD), Scanning electron microscope (SEM), Thermal gravimetric analysis (TGA), and Vibratingsample magnetometer (VSM) techniques. Particle size was below 200 nm and zeta potential was within the limit for all the batches. UV visible spectra at 224 nm, and FTIR exhibit two peaks at 510 and 594 cm -1, indicating iron oxide NPs and XRD confirmed the crystalline nature of Fe. SEM showed a spherical shape for all batches. The use of a combination of ferric and ferrous is more effective than its individual use. TGA and VSM studies confirmed its magnetic properties.
引用
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页码:1 / 8
页数:8
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