Comparison of different approaches of soil sampling uncertainty determination

被引:7
作者
Glavic-Cindro, Denis [1 ]
Bruggeman, Michel [2 ]
Crnic, Bostjan [1 ]
Necemer, Marijan [1 ]
Petrovic, Toni [1 ]
Prem, Petra [1 ]
Vodenik, Branko [1 ]
Zorko, Benjamin [1 ]
机构
[1] Joz ef Stefan Inst, Jamova Cesta 39, Ljubljana SI-1000, Slovenia
[2] Belgian Nucl Res Ctr SCK CEN, Boeretang 200, B-2400 Mol, Belgium
关键词
Radioactivity; Sampling; Soil samples; Uncertainty; Sampling uncertainty; Uncertainty budget; High resolution gamma-ray spectrometry; Environmental samples; Radionuclides; ANOVA; Between-sample variance; Between-analysis variance; ISO; IEC; 17025; 2017; GAMMA-RAY SPECTROMETRY;
D O I
10.1016/j.apradiso.2023.110676
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The ISO/IEC 17025 standard requires that all significant contributions have to be propagated to the measurement uncertainty, including also sampling uncertainties. We evaluated soil sampling uncertainties for gamma-ray spectrometry by using in-house and split-sample methods. By in-house method, the sampling uncertainty was determined by comparing standard deviations of measurement results and average analytical uncertainty. With split-sample method, it was calculated using between-sample and between-analysis variances. If analytical un-certainty is reliably determined, the in-house method is recommended because fewer measurements are needed.
引用
收藏
页数:8
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