In-situ Raman study of ?-D-glucose under different pressure and temperature

被引：4

作者：

Zheng, Zhenhong ^{[1
]}

Yao, Xueshuang ^{[1
]}

Zhang, Sinan ^{[1
]}

Fang, Leiming ^{[2
]}

Jiang, Zhuo ^{[1
]}

机构：

[1] South China Agr Univ, Coll Food Sci, Wushan Rd, Guangzhou 510640, Peoples R China

[2] China Acad Engn Phys, Key Lab Neutron Phys, Mianyang 621000, Peoples R China

来源：

JOURNAL OF MOLECULAR STRUCTURE | 2023年 / 1274卷

基金：

中国国家自然科学基金;

关键词：

High pressure; In-situ; Raman spectroscopy; Molecular structure; α -D-glucose; FOURIER-TRANSFORM RAMAN; INFRARED-SPECTROSCOPY; HYDROGEN-BONDS; SPECTRA; OLIGOSACCHARIDES; FRUCTOSE; CRYSTAL; HONEY;

D O I：

10.1016/j.molstruc.2022.134539

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

High-pressure Raman and infra-red spectroscopies were employed to explore how the molecular struc-ture of alpha-D-glucose changes under high pressure and temperature. At room temperature, the spectra show a significant pressure dependence and changed abruptly in the 5.7-5.9 GPa pressure range. The spectra of alpha-D-glucose crystals did not change significantly when the temperature was raised from 25 degrees C to 110 degrees C. However, the synergistic effect of temperature and pressure could reduce the pressure to 4.4 GPa, indicating that high temperature may accelerate the change of the molecular structure.(c) 2022 Elsevier B.V. All rights reserved.

引用

页数：10

共 36 条

[1] FT-Raman spectroscopic simultaneous determination of fructose and glucose in honey [J].

Batsoulis, AN ;

Siatis, NG ;

Kimbaris, AC ;

Alissandrakis, EK ;

Pappas, CS ;

Tarantilis, PA ;

Harizanis, PC ;

Polissiou, MG .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2005, 53 (02) :207-210

[2] A complete characterization of the vibrational spectra of sucrose [J].

Beatriz Brizuela, Alicia ;

Cecilia Bichara, Laura ;

Romano, Elida ;

Yurquina, Alisia ;

Locatelli, Silvano ;

Antonia Brandan, Silvia .

CARBOHYDRATE RESEARCH, 2012, 361 :212-218

[3] High-pressure diffraction studies of molecular organic solids. A personal view [J].

Boldyreva, Elena V. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :218-231

[4] Hydrogen Bond Length as a Key To Understanding Sweetness [J].

Bruni, F. ;

Di Mino, C. ;

Imberti, S. ;

McLain, S. E. ;

Rhys, N. H. ;

Ricci, M. A. .

JOURNAL OF PHYSICAL CHEMISTRY LETTERS, 2018, 9 (13) :3667-3672

[5] FOURIER-TRANSFORM RAMAN STUDIES OF MATERIALS AND COMPOUNDS OF BIOLOGICAL IMPORTANCE .2. THE EFFECT OF MOISTURE ON THE MOLECULAR-STRUCTURE OF THE ALPHA-ANOMERS AND BETA-ANOMERS OF D-GLUCOSE [J].

CORBETT, EC ;

ZICHY, V ;

GORAL, J ;

PASSINGHAM, C .

SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 1991, 47 (9-10) :1399-1411

[6] Fourier transform Raman spectroscopy of honey [J].

de Oliveira, LFC ;

Colombara, R ;

Edwards, HGM .

APPLIED SPECTROSCOPY, 2002, 56 (03) :306-311

[7] THE QSAR PREDICTION OF MELTING-POINT, A PROPERTY OF ENVIRONMENTAL RELEVANCE [J].

DEARDEN, JC .

SCIENCE OF THE TOTAL ENVIRONMENT, 1991, 109 :59-68

[8] Solid State Mutarotation of Glucose [J].

Dujardin, N. ;

Dudognon, E. ;

Willart, J. -F. ;

Hedoux, A. ;

Guinet, Y. ;

Paccou, L. ;

Descamps, M. .

JOURNAL OF PHYSICAL CHEMISTRY B, 2011, 115 (07) :1698-1705

[9] Complementarity of Raman and Infrared Spectroscopy for Structural Characterization of Plant Epicuticular Waxes [J].

Farber, Charles ;

Li, Jingbai ;

Hager, Elizabeth ;

Chemelewski, Robert ;

Mullet, John ;

Rogachev, Andrey Yu. ;

Kurouski, Dmitry .

ACS OMEGA, 2019, 4 (02) :3700-3707

[10] Progress toward the rapid nondestructive assessment of the floral origin of European honey using dispersive Raman spectroscopy [J].

Goodacre, R ;

Radovic, BS ;

Anklam, E .

APPLIED SPECTROSCOPY, 2002, 56 (04) :521-527

← 1 2 3 4 →