A novel synthesis of hollow Fe3O4 nanorods with a high saturation magnetization

被引:2
作者
Long, Zhimei [1 ]
Li, Chaoqun [1 ,2 ]
Zhang, Qingqing [1 ]
Xie, Wanyue [3 ]
Ma, Yilong [1 ]
Li, Kejian [1 ]
Guo, Donglin [1 ]
Shao, Bin [1 ,3 ]
机构
[1] Chongqing Univ Sci & Technol, Coll Met & Mat Engn, Chongqing 401331, Peoples R China
[2] Hangzhou Kede Magnet Components Co Ltd, Hangzhou 311500, Peoples R China
[3] Chongqing Acad S&T Dev, Chongqing 401331, Peoples R China
基金
中国国家自然科学基金;
关键词
Fe3O4; Nanorod; Hollow; Magnetic property; Nanoparticle; Magnetic materials; FEOOH NANORODS; ONE-POT; TRANSFORMATION; NANOSTRUCTURES;
D O I
10.1016/j.matlet.2023.135301
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A novel approach combined Stober method with the hydrothermal method was developed for the synthesis of hollow Fe3O4 nanorods by using SiO2 as the template and FeOOH nanorods as the precursor. The investigation of the reaction process confirmed that, as the SiO2 outer layer was gradually dissolved and partially nitrided to Si3N4 in an alkaline hydrazine solution, FeOOH was converted to Fe3O4, resulting in a regular rod-shaped morphology with a hollow structure. The prepared hollow Fe3O4 nanorods had an average length of 430 nm and an average width of 110 nm, and exhibited a high saturation magnetization of 81.6 emu g(-1).
引用
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页数:4
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