Impact of the Calcination Temperature on Structural, Electrical and Dielectric Properties for Mg0.6Cu0.4FeCrO4 Spinel Ferrites

被引:4
|
作者
Jdey, Warda [1 ]
Mzoughi, Thabet [1 ]
Hamdaoui, Nejeh [1 ,2 ]
Hcini, Sobhi [3 ]
Mansouri, Salaheddine [3 ]
机构
[1] Univ Sousse, Higher Sch Sci & Technol Hammam Sousse, Lab Energy & Mat LabEM LR11ES34, St Lamine Abbassi, Hammam Sousse 4011, Tunisia
[2] Univ Sousse, ISITCom, Higher Inst Comp Sci & Commun Technol Hammam Souss, Gp1, Hammam Sousse 4011, Tunisia
[3] Univ Kairouan, Fac Sci & Technol Sidi Bouzid, Sidi Bouzid 9100, Tunisia
关键词
Spinel ferrite; Sol-gel method; Sintering temperature; Structural properties; Impedance spectroscopic properties; CATION DISTRIBUTION; MAGNETIC-PROPERTIES; MAGNETOCALORIC PROPERTIES; PHYSICAL-PROPERTIES; NANO-FERRITES; NI; NANOPARTICLES; MOSSBAUER; SUBSTITUTION; SPECTROSCOPY;
D O I
10.1007/s10904-023-02763-0
中图分类号
O63 [高分子化学(高聚物)];
学科分类号
070305 ; 080501 ; 081704 ;
摘要
During this work, we synthesize Mg0.6Cu0.4FeCrO4 powders by the sol-gel method, and then we sinter this powders prepared at two different temperatures (900 & DEG;C and 1100 & DEG;C). Structural analysis was studied by X-ray diffraction (XRD) and Rietveld refinement show a single pure phase with cubic spinel structure (Fd-3m). The behavior of constants dielectrics for both samples shows giant values for the real (& epsilon;& PRIME; & AP; 10(3) and & epsilon;& PRIME; & AP; 10(4), respectively, for s900 and s1100) and imaginary (& epsilon;& DPRIME; & AP; 10(4) and & epsilon;& PRIME; & AP; 10(6), respectively, for s900 and s1100) part of the permittivity. By analyzing the relaxation time and ac-conductivity, it was discovered that the same type of charge carriers may be responsible for both the relaxation and conduction processes.
引用
收藏
页码:3485 / 3500
页数:16
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