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Impact of the Calcination Temperature on Structural, Electrical and Dielectric Properties for Mg0.6Cu0.4FeCrO4 Spinel Ferrites
被引:4
|作者:
Jdey, Warda
[1
]
Mzoughi, Thabet
[1
]
Hamdaoui, Nejeh
[1
,2
]
Hcini, Sobhi
[3
]
Mansouri, Salaheddine
[3
]
机构:
[1] Univ Sousse, Higher Sch Sci & Technol Hammam Sousse, Lab Energy & Mat LabEM LR11ES34, St Lamine Abbassi, Hammam Sousse 4011, Tunisia
[2] Univ Sousse, ISITCom, Higher Inst Comp Sci & Commun Technol Hammam Souss, Gp1, Hammam Sousse 4011, Tunisia
[3] Univ Kairouan, Fac Sci & Technol Sidi Bouzid, Sidi Bouzid 9100, Tunisia
关键词:
Spinel ferrite;
Sol-gel method;
Sintering temperature;
Structural properties;
Impedance spectroscopic properties;
CATION DISTRIBUTION;
MAGNETIC-PROPERTIES;
MAGNETOCALORIC PROPERTIES;
PHYSICAL-PROPERTIES;
NANO-FERRITES;
NI;
NANOPARTICLES;
MOSSBAUER;
SUBSTITUTION;
SPECTROSCOPY;
D O I:
10.1007/s10904-023-02763-0
中图分类号:
O63 [高分子化学(高聚物)];
学科分类号:
070305 ;
080501 ;
081704 ;
摘要:
During this work, we synthesize Mg0.6Cu0.4FeCrO4 powders by the sol-gel method, and then we sinter this powders prepared at two different temperatures (900 & DEG;C and 1100 & DEG;C). Structural analysis was studied by X-ray diffraction (XRD) and Rietveld refinement show a single pure phase with cubic spinel structure (Fd-3m). The behavior of constants dielectrics for both samples shows giant values for the real (& epsilon;& PRIME; & AP; 10(3) and & epsilon;& PRIME; & AP; 10(4), respectively, for s900 and s1100) and imaginary (& epsilon;& DPRIME; & AP; 10(4) and & epsilon;& PRIME; & AP; 10(6), respectively, for s900 and s1100) part of the permittivity. By analyzing the relaxation time and ac-conductivity, it was discovered that the same type of charge carriers may be responsible for both the relaxation and conduction processes.
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页码:3485 / 3500
页数:16
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