Copper-catalyzed one-pot synthesis of 1,4-benzothiazine-3-ones

被引：1
|
作者：
Zhang, Lingyu [1 ]
Zhang, Songlin [1 ]
机构：
[1] Soochow Univ, Coll Chem Chem Engn & Mat Sci, Key Lab Organ Synth Jiangsu Prov, Suzhou 215123, Peoples R China
来源：
TETRAHEDRON LETTERS | 2023年 / 130卷
基金：
中国国家自然科学基金;
关键词：
Copper catalyst; Cross-coupling; Nitrogen heterocycles; Ullmann reaction; 4-Benzothiazin-3-ones; C-N; DERIVATIVES; EFFICIENT; CHEMISTRY; BROMIDES;
D O I：
10.1016/j.tetlet.2023.154761
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An efficient potassium carbonate and copper-mediated C-S and C-N Ullmann coupling reaction between 2-bromothiophenol and 2-haloacetanilide is reported here. This protocol affords a simple and efficient approach for the construction of 1,4-benzothiazinone-3-one derivatives, avoiding the limitations of using noble metals and expensive ligands for the first time.
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页数：4
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