Emerging procedures and solvents in biological sample pre-treatment

被引:10
|
作者
Greco, Valentina [1 ]
Giuffrida, Alessandro [1 ]
Locatelli, Marcello [2 ]
Savini, Fabio [3 ]
de Grazia, Ugo [4 ]
Ciriolo, Luigi [2 ]
Perrucci, Miryam [2 ]
Kabir, Abuzar [5 ]
Ulusoy, Halil Ibrahim [6 ]
D'Ovidio, Cristian [7 ]
Maria, Antonio [8 ]
Ali, Imran [9 ]
机构
[1] Univ Catania, Dept Chem Sci, Viale Andrea Doria 6, I-95125 Catania, Italy
[2] Univ Chieti Pescara G Annunzio, Dept Pharm, Via Vestini 31, I-66100 Chieti, Italy
[3] Hosp St Spirito, Pharmatoxicol Lab, Via Fonte Romana 8, I-65124 Pescara, Italy
[4] Fdn IRCCS Ist Neurol Carlo Besta, Lab Neurol Biochem & Neuropharmacol, Via Celoria 11, I-20133 Milan, Italy
[5] Florida Int Univ, Int Forens Res Inst, Dept Chem & Biochem, Miami, FL 33199 USA
[6] Cumhuriyet Univ, Fac Pharm, Dept Analyt Chem, TR-58140 Sivas, Turkiye
[7] Univ Chieti Pescara G Annunzio, Dept Med & Aging Sci, Sect Legal Med, I-66100 Chieti, Italy
[8] Univ Rome 2 Tor Vergata, Inst Legal Med, I-00133 Rome, Italy
[9] Jamia Millia Islamia, Dept Chem, New Delhi 110025, India
来源
ADVANCES IN SAMPLE PREPARATION | 2023年 / 6卷
关键词
Bioanalytic; Drug stability; Toxicological; Forensic; Biological matrices; Additives and stabilizers; LC-MS/MS; STABILITY; ENZYMES; PLASMA; DEGRADATION; DOXORUBICIN; DRUGS; STABILIZATION; BIOSAMPLES; COLLECTION;
D O I
10.1016/j.sampre.2023.100066
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The treatment of biological samples, especially from complex matrices, has consistently challenged analytical operators. The classic problems to be faced for any analysis, regardless of the origin of the sample, such as for example contamination and loss of analyte, in biological samples, are particularly emphasized. In particular, the main cause of the error is due to the degradation of the analyte which in several cases due to biological inter-action. Many factors can influence the stability of drugs, chief among them the physicochemical properties of the drug, characteristics of the matrix, the tendency to conjugation/deconjugation, sample collection procedure, container characteristics (e.g., oxidation, adsorption), and the use of preservatives or other additives. The prob-lem is severe in the toxicological and forensic fields, especially for analyzes considered "non-repeatable." In this review, we will explore all the major problems in the pre-extraction phase for the chemical-analytical aspect in the pharmacotoxicological and forensic fields.
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页数:8
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