UPLC-Q-TOF/MS analysis of chemical constituents of methanolic extract from cassava tender stems

被引:0
作者
Zhang, J. [1 ]
Ye, J. Q. [1 ]
Xiao, X. H. [1 ]
Wang, M. [1 ]
Li, K. M. [1 ]
Chen, J. [2 ,3 ,4 ]
机构
[1] Chinese Acad Trop Agr Sci, Inst Trop Crop Genet Resources, Haikou 571101, Peoples R China
[2] Hainan Univ, Key Lab Food Nutr & Funct Food Hainan Prov, Haikou 570228, Peoples R China
[3] Hainan Univ, Engn Res Ctr Utilizat Trop Polysaccharide Resource, Minist Educ, Haikou 570228, Peoples R China
[4] Hainan Univ, Coll Food Sci & Technol, Haikou 570228, Peoples R China
来源
INTERNATIONAL FOOD RESEARCH JOURNAL | 2023年 / 30卷 / 04期
关键词
cassava tender stem; liquid chromatography; mass spectrometry; chemical composition;
D O I
10.47836/ifrj.30.4.09
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
In the processing and utilisation of cassava, stems and leaves usually become waste. The tender stems of cassava were analysed by electrospray ionisation high-performance liquid chromatography-tandem mass spectrometry. Using UPLC BEH C18 column (50 x 2.1 mm; i.d.: 1.7 & mu;m), the mobile phases were H2O (0.1% FA) and CH3CN (0.1% FA), the column temperature was 30 & DEG;C, and the flow rate was 0.30 mL/min. Mass spectrometry was performed by the Waters SYNAPT G2 HDMS system. This gave excellent reproducibility and avoided the interference of some similar substances. A total of 33 compounds were identified in Bzhe samples of cassava tender stems by this method, mainly cyanosides, catechins, flavonoids, glycosides, glycosides, phospholipids, and other components. The present work provided reference value for the development and utilisation of cassava tender stems.
引用
收藏
页码:913 / 923
页数:11
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