Modernized Liquid Helium-Free Closed-Cycle Cryostat for Mossbauer Research

被引:3
作者
Starchikov, S. S. [1 ]
Funtov, K. O. [1 ]
Zayakhanov, V. A. [1 ]
Frolov, K. V. [1 ]
Klenov, M. G. [2 ]
Bondarenko, I. Yu. [2 ]
Lyubutin, I. S. [1 ]
机构
[1] Russian Acad Sci, Shubnikov Inst Crystallog, Fed Sci Res Ctr Crystallog & Photon, Moscow 119333, Russia
[2] OOO CryoPribor, Moscow 123060, Russia
基金
俄罗斯基础研究基金会;
关键词
NANOPARTICLES; SPECTROSCOPY; SPECTRA;
D O I
10.1134/S0020441223020239
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
One of the problems in the use of closed-cycle cryostats for applied and basic scientific research is the transmission of mechanical vibrations to the sample. This is particularly relevant for Mossbauer spectroscopy and optical research methods since vibrations lead to broadening of spectral lines. This paper presents various engineering approaches to reducing mechanical vibrations on a sample in closed-cycle cryostats, in particular for Mossbauer spectroscopy. The broadening of the spectral lines of the reference absorber, & alpha;-Fe foil, was analyzed and a comparison of the spectra of a FeBO3 single crystal of high structural quality before and after updating the cryostat was made. The obtained results can be used to develop new cryostats or improve existing ones.
引用
收藏
页码:497 / 507
页数:11
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