Dispersive solid-phase extraction for the determination of organochlorine pesticides in fruit juice samples using iron-doped zinc oxide nanoparticles supported with silica as a sorbent

被引:3
作者
Tesfaye, Bereket [1 ,2 ]
Gure, Abera [1 ]
Asere, Tsegaye Girma [1 ]
Teshome, Toleshi [1 ]
Buzayo, Yerosan [1 ]
机构
[1] Jimma Univ, Coll Nat Sci, Dept Chem, Jimma, Ethiopia
[2] Jimma Univ, Coll Nat Sci, Dept Chem, POB 378, Jimma, Ethiopia
关键词
dispersive solid phase extraction; fruit juices; gas chromatography-mass spectroscopy; iron-doped zinc oxide nanoparticles; organochlorine pesticides; PERFORMANCE LIQUID-CHROMATOGRAPHY; MULTIRESIDUE METHOD; RESIDUES; WATER; MICROEXTRACTION; HERBICIDES; HONEY; TRENDS; FOOD;
D O I
10.1002/sscp.202300161
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An efficient analytical method has been developed based on dispersive solid-phase extraction followed by gas chromatography-mass spectrometry for the determinations of 13 organochlorine pesticides in fruit juice samples. In this method, dispersive solid phase extraction was used for the extraction of target analye using iron-doped zinc oxide nanoparticles supported with silica as a sorbent. Different experimental parameters affecting the extraction efficiencies the proposed method were carefully optimized. Under the optimum conditions, the calibration graphs were linear in the concentration range of 0.6-100 ng/mL with coefficients of determinations in the range of 0.9927-0.9991. The limits of detection and quantification determined as 3 and 10 times the signal-to-noise ratio were in the range of 0.01-0.03 and 0.6-1.0 ng/mL, respectively. Intra- and inter-day precision studies of the proposed method, expressed as relative standard deviations, were in the range of 2.1%-9.2% and 2.2%-9.7%, respectively. The recoveries of the spiked fruit juices samples were in the range of 81.4%-105.1% with the corresponding relative standard deviations ranging from 1.0%-8.8%. In general, the proposed method demonstrated satisfactory analytical performance. Thus,it could be used as simple and attracive alternative method for the extraction of organochlorine pesticides from fruit juice sample and other related matrices.
引用
收藏
页数:11
相关论文
共 40 条
  • [1] Anastassiades M., 2003, Journal of AOAC International, V86, P412
  • [2] Graphene-based Magnetic Solid Phase Extraction-Dispersive Liquid Liquid Microextraction Combined with Gas Chromatographic Method for Determination of Five Acetanilide Herbicides in Water and Green Tea Samples
    Bai Sha-Sha
    Li Zhi
    Zang Xiao-Huan
    Wang Chun
    Wang Zhi
    [J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2013, 41 (08) : 1177 - 1182
  • [3] Fast and simple extraction of pesticide residues in selected fruits and vegetables using tetrafluoroethane and toluene followed by ultrahigh-performance liquid chromatography/tandem mass spectrometry
    Bakirci, Gozde Turkoz
    Hisil, Yasar
    [J]. FOOD CHEMISTRY, 2012, 135 (03) : 1901 - 1913
  • [4] Quantitative analysis of flavanones from citrus fruits by using mesoporous molecular sieve-based miniaturized solid phase extraction coupled to ultrahigh-performance liquid chromatography and quadrupole time-of-flight mass spectrometry
    Cao, Wan
    Ye, Li-Hong
    Cao, Jun
    Xu, Jing-Jing
    Peng, Li-Qing
    Zhu, Qiong-Yao
    Zhang, Qian-Yun
    Hu, Shuai-Shuai
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2015, 1406 : 68 - 77
  • [5] Dispersive Solid-Phase Extraction of Polyphenols from Juice and Smoothie Samples Using Hybrid Mesostructured Silica Followed by Ultra-high-Performance Liquid Chromatography-Ion-Trap Tandem Mass Spectrometry
    Casado, Natalia
    Morante-Zarcero, Sonia
    Perez-Quintanilla, Damian
    Camara, Jose S.
    Sierra, Isabel
    [J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2019, 67 (03) : 955 - 967
  • [6] Dispersive micro-solid phase extraction
    Chisvert, Alberto
    Cardenas, Soledad
    Lucena, Rafael
    [J]. TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2019, 112 : 226 - 233
  • [7] Recent Advances and Trends in Applications of Solid-Phase Extraction Techniques in Food and Environmental Analysis
    Faraji, Mohammad
    Yamini, Yadollah
    Gholami, Mehrnoosh
    [J]. CHROMATOGRAPHIA, 2019, 82 (08) : 1207 - 1249
  • [8] Dispersive solid phase extraction based on simply prepared nitrogen-doped amorphous carbon nanocomposite combined with dispersive liquid-liquid microextraction: application in the extraction of some pesticides from fruit juices
    Farajzadeh, Mir Ali
    Davaran, Maryam
    Mohebbi, Ali
    Afshar Mogaddam, Mohammad Reza
    [J]. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2021, 18 (08) : 2151 - 2164
  • [9] Multiresidue analysis of organochlorine and organophosphorus pesticides in muscle of chicken, pork and lamb by gas chromatography-triple quadrupole mass spectrometry
    Frenich, AG
    Vidal, JLM
    Sicilia, ADC
    Rodríguez, MJG
    Bolaños, PP
    [J]. ANALYTICA CHIMICA ACTA, 2006, 558 (1-2) : 42 - 52
  • [10] Preparation and sedimentation behavior in magnetic fields of magnetite-covered clay particles
    Galindo-González, C
    de Vicente, J
    Ramos-Tejada, MM
    López-López, MT
    González-Caballero, F
    Durán, JDG
    [J]. LANGMUIR, 2005, 21 (10) : 4410 - 4419