Synthesis, analysis and characterization of camellia sinensis mediated synthesis of NiO nanoparticles for ethanol gas sensor applications

被引:30
作者
Ananthi, S. [1 ]
Kavitha, M. [1 ]
Balamurugan, A. [2 ]
Kumar, E. Ranjith [3 ]
Magesh, G. [4 ]
Abd El-Rehim, A. F. [5 ]
Srinivas, Ch. [6 ]
Anilkumar, P. [7 ]
Suryakanth, J. [3 ]
Rahale, C. Sharmila [8 ]
机构
[1] Madura Coll, Dept Phys, Madurai 625011, Tamil Nadu, India
[2] Govt Arts & Sci Coll, Dept Phys, Avinashi 641654, Tamil Nadu, India
[3] KPR Inst Engn & Technol, Dept Phys, Coimbatore 641407, Tamil Nadu, India
[4] Thiruvalluvar Coll, Dept Phys, Tirunelveli 627425, Tamil Nadu, India
[5] King Khalid Univ, Fac Sci, Phys Dept, POB 9004, Abha 61413, Saudi Arabia
[6] Sasi Inst Technol & Engn, Dept Phys, Nanomat & Nanomagnetism Res Lab, Tadepalligudem 534101, Andhra Pradesh, India
[7] KPR Inst Engn & Technol, Dept Chem, Coimbatore 641407, Tamil Nadu, India
[8] Tamil Nadu Agr Univ, Ctr Agr Nanotechnol, Coimbatore, Tamilnadu, India
来源
SENSORS AND ACTUATORS B-CHEMICAL | 2023年 / 387卷
关键词
Green synthesis; Metal oxide nanoparticles; Structural studies; Zeta potential; Ethanol sensor; PULSED-LASER ABLATION; GREEN SYNTHESIS; NANOSTRUCTURES;
D O I
10.1016/j.snb.2023.133742
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A green combustion technique assisted by freshly extracted tea (Camellia sinensis /natural tannic acid) was adopted to synthesize NiO nanoparticles. Further research into the physicochemical properties of the NiO nanoparticles was conducted after heating them to 350 celcius. The average particle size of NiO nanoparticles in their as-prepared state was found to be 18.4 nm, while the average particle size of NiO nanoparticles in their heat-treated condition was found to be 28.7 nm. The scanning electron microscope (SEM) and transmission elec-tron microscope (TEM) were used to record NiO nanoparticles' external morphology, particle shape, and particle size. It was discovered that the NiO nanoparticles had a spherical shape with an average particle size of 26 nm for the samples created as is and 35 nm for the heated samples. The performance assessment of the petrol sensor was carried out using a number of testing techniques and a variety of gases. NiO nanoparticles outperformed all other testing gases when it came to how effectively the sensor responded to ethanol gas. NiO nanoparticles are interesting materials for use in gas sensor applications, as evidenced by their response-recovery time.
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页数:9
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